5975C GC/MSD
5975C GC/MSD Agilent 5975C GC/MSD GC/MS 5975C GC/ MSD HED-EM 5975C MSD 789A GC 5975C GC/ MSD 2
Time > 12.8 13. 13.2 Time > 12.8 13. 13.2 5975C GC/MSD Inert Ion Source 125 9 8 19 7 6 5 4 3 79 93 2 63 1 5 138 15 169182 21 2 m/z > 4 6 8 1 12 14 16 18 2 2 GC/MS back flush 5 35 6 Enhanced Signal hexachlorobi Triple-Axis de Off-Axis dete 5975C GC/MSD 2 6 TAD 7 DRS 5975C GC/MSD GC/ MS / GC/MS 1 1 5989-6351CHCN 5975C GC/ MSD N 2 He H 2 4 2 3 Linear velocity (cm/sec) Adduct ions LOD 7 SIM/Scan 125 u/s 8 MS MS 8 PCI NCI CI PCI NCI 9 GC/MS 1 DRS 1 Agilent 5975C GC/MSD www.agilent.com/chem/5975c 3
789A GC 4 789A GC GC/MS 789A GC/MS 789A GC GC/MS GC GC/MS 789A GC EPC MMI MMI 4
RTL RTL Abundance A: TIC: lettuce_blank.d\data.ms B: TIC: lettuce_blank3.d\data.ms 4e+7 789A EPC RTL 3e+7 2e+7 1e+7 B A RTL GC/MSD RTL Time 4. 6. 8. 1. 12. 14. 16. 18. 2. Overlapped chromatograms of a blank extract injected before A and after B three injections without backflush. CFT Abundance 4.6e+7 4.4e+7 4.2e+7 4e+7 3.8e+7 3.6e+7 3.4e+7 3.2e+7 3e+7 2.8e+7 2.6e+7 2.4e+7 2.2e+7 2e+7 1.8e+7 1.6e+7 1.4e+7 1.2e+7 1e+7 TIC: Lettuce_1_ppb.D\data.ms TIC: Lettuce_1_ppb.D\data.ms TIC: Lettuce_5_ppb.D\data.ms Time 4. 6. 8. 1. 12. 14. 16. 18. 2. Overlapped chromatogram of three lettuce extracts run with 2 minutes of backflush. No analyses without backflush were run between them. Ultimate Union PPU GC Agilent 5975C GC/MSD www.agilent.com/chem/5975c 5
GC/MS 35 C EI 2 Inert Ion Source 125 277 9 8 19 7 6 26 5 4 3 79 93 2 63 1 5 138 15 169182 214 247 2 228 m/z > 291 315 327 4 6 8 1 12 14 16 18 2 22 24 26 28 3 32 Stainless Steel Ion Source 125 9 247 8 19 138 277 7 6 5 26 4 79 3 93 2 63 1 5 152 169 182 2 214 23 295 38327339 m/z > 4 6 8 1 12 14 16 18 2 22 24 26 28 3 32 MSD MSD 2 C 15 u PBDEs 3 2 5989-651EN: 5975C MSD 3 5989-3142EN: 5975 Inert MSD PBDEs, 138 u 247 u 6
TAD 5975C EM TID TID MDL LOQ 18.8 218.9 Abundance 57. 83. 11.9 Abundance Enhanced Signal hexachlorobiphenyl @ 25 fg Triple-Axis detector S/N-rms: 25 Off-Axis detector S/N-rms: 35 3 2 146. 252.9 1 281. 331. 417.4 Time > 12.8 13. 13.2 m/z > 6 8 1 12 14 16 18 2 22 24 26 28 3 32 34 36 38 4 42 Time > Reduced neutral noise Abundance 3 182.8 218.8 TAD 2 111. 5975C AutoTune, EM 4 1 253.8 281. 331. 42.6 Time > 12.8 13. 13.2 m/z > 6 8 1 12 14 16 18 2 22 24 26 28 3 32 34 36 38 4 42 a- TID 51. 83. TID 145. 4 5989-7654EN: Agilent 5975C GC/MSD www.agilent.com/chem/5975c 7
SIM/Scan 5975C GC/MS SIM SIM/ Scan 5 Scan SIM SIM/Scan Performance Electronics 6,25 u/sec More Signal SIM Mode: 1x lower.1 ng Cocaine and 2 ng Arachidonic Standard Electronics 6,25 u/sec.84 sec width half height Abundance 35 25 15.1 ng Cocaine 77 Q2 94 Q3 82 T 182 Q1 At 1x lower analyte, Q2 and Q3 are lost in interference Biggest ions mode 82,182,77,94 SIM 5 7.6 7.62 7.64 7.66 7.68 7.55 7.6 7.65 7.7 Time 8.6 8.8 9. 9.2 9.4 9.6 9.8 1, Agilent 5973 MSD 125 u/sec Abundance 18 14 1 6 182 T 33 Q1 198 Q3 272 Q2 Use of higher selectivity ions makes quant and qualifiers easier to find Opt 7% 182,33,272,198 SIM 2 5975C GC/MSD GC/ MS Time 8.6 8.8 9. 9.2 9.4 9.6 9.8 1 5 5989-318EN: SIM/Scan 8
CI EI CI CI CI EI CI CI PCI ECNI CI EI THCA-PFPA-HFIP EI Spectrum MW=64 THCA-PFPA-HFIP PCI NH 3 Spectrum MW=64 658 PCI NCI ECNI CI Adduct ions 641 477 22 24 26 28 3 32 34 36 38 4 42 44 46 48 5 52 54 56 58 6 62 64 66 THCA-PFPA-HFIP NCI CH 4 Spectrum MW=64 62 472 492 36 235 283 383 34 432 452 64 6 24 26 28 3 32 34 36 38 4 42 44 46 48 5 52 54 56 58 6 62 64 THCA EI PCI NCI CI GC/MSD Agilent 5975C GC/MSD www.agilent.com/chem/5975c 9
GC/MS Productivity MSD Productivity 6 5975C GC/MSD PC GC/MS MSD GC RTL LIMS AutoQuant SIM SIM/ Scan AutoSIM RTL 2 4 2 MS / GC 7 SemiQuant 8 Enhanced EnviroQuant USEPA, DrugQuant ASTM MSD 9 FDA 21 CFR Part 11 DRS DRS GC/MSD QEdit MSD AMDIS NIST AMDIS1 NIST 17 CDFA 8 17 DRS 3 99 1 6 7 8 CDFA 37 DRS 37 99 1 1 8 32 min 5989-5219CHCN: GC GC/MSD MSDProductivity 5989-6115EN: GC GC/MSD MSD Productivity 5989-4997CHCN: SemiQuant: GC/MS ; 599-4164CHCN: Mass Profiler Professional 9 5989-522EN: GC/MS MSD Security ChemStation 1 5989-576CHCN: GC/MS 926 1
MassHunter MassHunter MS GC/MSD MassHunter OpenLAB ECM OpenLAB ECM 11 OpenLAB ECM 11 5989-614EN: GC/MSD OpenLAB ECM 11 Agilent 5975C GC/MSD www.agilent.com/chem/5975c
GC/MSD Agilent 5975C GC/MSD 2 EM EM SIM EM EMF GC MSD GC/MSD 12
GC/MS GC/MS 5975C GC/MSD 24 GC/MS EI, CI, MS/ MS, MS n EI CI 5975E GC/MSD 782A GC GC/ MSD GC/MS 22 GC/MS CI MS/MS 5975T LTM GC/MSD LTM Customized to get you on the FAST TRACK GC/MS 6 7 GC/ MS GC fg 5 / (MRM) GC/MS www.agilent.com/chem/gcms 13
5975C 7693A 7693A 7693A ALS 7693A 5975C CTC PAL CTC PAL GC GC/MS CombiPAL SPME GC PAL CombiPAL LVI 7697A 7697A 7697A, GC GC 7696A 7696A - 7696A HPLC LC/MS GC GC/MS 2 ml LC GC 14
GC/MS GC J&W GC 4 J&W GC / / GC GC/MS QuEChERS SPE Bond Elut Plexa Captiva O O J&W GC J&W GC J&W GC VF-ms Factor Four, DB-ms HP-ms J&W Select GC J&W LTM 5975T LTM GC/MSD 789 LTM www.agilent.com/chem/supplies 15
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