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1 玩具产业协会 New Lead and Heavy Elements Requirements: How to Test for Compliance 铅和重金属含量的新要求 : 如何测试是否符合规定 Alan P. Kaufman Senior Vice-President, Technical Affairs 技术事务高级副总裁 Toy Industry Association 玩具产业协会 August 1 & 3, 2012 Dongguan/Shenzhen, China 8 月 1 日东莞 8 月 3 日深圳

2 CPSIA Lead Limits How to Test 消费品安全改进法案规定的铅含量上限如何进行测试 Paints, inks and similar surface coatings limited to 90ppm 油漆墨水和其他类似表面涂层的铅含量上限为 90ppm Substrates limited to 100ppm 基材的铅含量上限为 100ppm These are both total limits (not soluble) 以上两者均为铅总含量上限 ( 不可溶解 ) Three standard CPSC methods: 美国消费品安全委员会的三项标准测试方法 : CPSC-CH-E Total Lead (Pb) in Metal Children s Products (including jewelry) CPSC-CH-E 儿童金属产品 ( 含首饰 ) 铅 (Pb) 总含量测试 CPSC-CH-E Total Lead (Pb) in Non-Metal Children s Products CPSC-CH-E 儿童非金属产品铅 (Pb) 总含量测试 CPSC-CH-E Total Lead (Pb) in Paint and Other Similar Surface Coatings CPSC-CH-E 油漆和其他类似表面涂层铅 (Pb) 总含量测试 Compositing is acceptable (up to three samples per composite) so long as procedure is such that no failure will go undetected 只要程序不会检测不出不合格的情况, 便可接受材料混测 ( 不能超过三个样品 ) Standard method is nitric acid digestion; acceptable analysis methods are flame AA, GFAA, ICP-OES, or ICP-MS 标准测试方法为硝酸消解 ; 可接受的分析方法为 Flame AA GFAA ICP-OES 或 ICP-MS 测试方法 XRF acceptable for homogeneous polymeric substrates; HD-XRF conforming to ASTM F acceptable for paints and surface coatings (proposed extension to glass, crystal, and some metals) 同质聚合物基材可以用 XRF 仪器进行测试 ; 油漆和表面涂层 ( 拟延伸至玻璃水晶和某些金属 ) 可以用与 ASTM F 相符的 HD-XRF 仪器进行测试 2

3 F Heavy Elements F 重金属 Updated to add CPSIA lead limits: 90ppm for surface coatings/100ppm for substrates 更新增加了消费品安全改进法案规定的铅含量上限 : 表面涂层为 90ppm/ 基材为 100ppm For the other heavy elements: Extends soluble element limitations to substrates (previously applied only to surface coatings) 其它重金属 : 增加了对基材的可溶性重金属的限值 ( 之前仅针对表面涂层 ) Adds option of total screen to demonstrate compliance with soluble limits 增加了重金属总含量的筛查法以证明符合可溶性限值 Adds test methods for substrate testing 增加了对基材进行测试的测试方法 Adds 24-hour cadmium migration test for metallic small parts; 200ug maximum extraction limit (if <75ppm total Cd in screening, not applicable) 针对金属小部件增加了 24 小时镉迁移测试 ; 溶出限值最大为 200ug( 如果在筛查时镉的总含量 <75ppm, 则不适用 ) Adds compositing procedure-compositing up to three samples explicitly allowed for total element testing (not for soluble) 增加了材料混测方式, 可用于进行重金属总含量测试 ( 不适用于可溶性测试 ), 并明确混料里最多允许三个样品 Standard is now essentially aligned with both EN71 and ISO 8124, except that F contains the additional CPSIA total lead and 24-hour cadmium requirements, and explicitly allows total screening test 除了 F 中载有额外的消费品安全改进法案规定的总含铅量以及 24 小时镉迁移测试的要求, 以及明确允许重金属总含量筛查测试之外, 本标准目前已基本与 EN71 和 ISO 8124 相一致 3

4 F Heavy Elements (cont) F 重金属 ( 续 ) Maximum Soluble Migrated Element in ppm (mg/kg) for Surface Coatings and Substrates Other Than Modeling Clay Included as Part of a Toy 玩具部件中, 除了造型粘土以外的表面涂层和基材的可溶性迁移重金属上限值单位 :ppm(mg/kg) Antimony Arsenic Barium Cadmium Chromium Lead Mercury Selenium 锑砷钡镉铬铅水银硒 (Sb) (As) (Ba) (Cd) (Cr) (Pb) (Hg) (Se) Maximum Soluble Migrated Element in ppm (mg/kg) for Modeling Clays Included as Part of a Toy 玩具部件中, 造型粘土的可溶性迁移重金属上限值单位 :ppm(mg/kg) Antimony Arsenic Barium Cadmium Chromium Lead Mercury Selenium 锑砷钡镉铬铅水银硒 (Sb) (As) (Ba) (Cd) (Cr) (Pb) (Hg) (Se)

5 F Heavy Elements (cont) F 重金属 ( 续 ) Paper and paperboard are not tested; 没有对纸或纸板进行测试 ; Fabrics and other material exempted by 16CFR and 16CFR also exempt from F963 total and soluble lead in substrate requirements (but subject to soluble limits for 7 other elements) 织物及其他材料不受 16CFR 和 16CFR 中要求的管制, 也不受 F963 中针对基材铅总含量及可溶性铅含量的要求 ( 但依然受到其他七大重金属可溶性限值的限制 ) Compositing not allowed for soluble element testing 可溶性重金属测试不允许采用材料混测方法 Surface coating limitations generally apply up to age 14 years; 表面涂层限值一般适用于针对 14 岁以下儿童的产品 ; Substrate requirements generally apply to: 对基材的要求一般适用于 : accessible components of items for under six years of age unless they cannot be mouthed, licked, or sucked; 6 岁以下儿童可接触到的玩具组件, 除非这些部件无法接触到嘴部或被舔吸 ; also to accessible components of products for ages up to 14 years intended to be mouthed (example: toy harmonica) or intended to come in contact with, or to store, food or drink; 用于 14 岁或以下儿童嘴部接触 ( 例如 : 玩具口琴 ) 的产品部件, 或是用于接触或储存食物或饮料的产品部件 ; toy writing instruments; play cosmetics; or products otherwise likely to be mouthed 玩具书写用品 ; 玩具化妆品或其他有可能与嘴部接触的产品 5

F963-11 How to test for Heavy Elements F963-11 如何测试重金属 Screen for all eight elements by total screen per appropriate CPSC test: 根据恰当的美国消费品安全委员会测试, 通过筛查重金属总含量对八大重金属进行筛查 : CPSC-CH-E1001-08.

6 F How to test for Heavy Elements F 如何测试重金属 Screen for all eight elements by total screen per appropriate CPSC test: 根据恰当的美国消费品安全委员会测试, 通过筛查重金属总含量对八大重金属进行筛查 : CPSC-CH-E Total Lead (Pb) in Metal Children s Products (including jewelry) CPSC-CH-E 儿童金属产品 ( 含首饰 ) 铅 (Pb) 总含量测试 CPSC-CH-E Total Lead (Pb) in Non-Metal Children s Products CPSC-CH-E 儿童非金属产品铅 (Pb) 总含量测试 CPSC-CH-E Total Lead (Pb) in Paint and Other Similar Surface Coatings CPSC-CH-E 油漆和其他类似表面涂料铅 (Pb) 总含量测试 If all results are below CPSIA total lead limits and all seven other elements are below applicable F soluble limits, testing is complete-item complies 如果所有测试结果均低于消费品安全改进法案铅总含量限值, 同时其它七大重金属含量均低于适用的 F 可溶性限值, 则测试完成产品合格 If total lead results are below CPSIA total lead limits but some or all results for other seven elements exceed applicable F soluble limits, proceed to test for soluble element content per ASTM F963-11, section 8.3; if all soluble results are below soluble limits, testing is complete-item complies 如果总铅含量测试结果低于消费品安全改进法案铅总含量限值, 但其它七大重金属含量的部分或所有测试结果超出了适用的 F 可溶性限值, 则继续按照 F 第 8.3 条来测试可溶性重金属含量 ; 如果全部可溶性结果均低于可溶性限值, 则测试完成产品合格 If CPSIA total lead limits are exceeded, or soluble limits are exceeded in soluble testing-item FAILS 如果超出了消费品安全改进法案铅总含量限值, 或超过了可溶性测试中的可溶性限值产品不合格 6

GB Sparkle

GB Sparkle GB 24613-2009 Chinese Mandatory Standard for Toy Coatings With growth of the toy industry and improvement of toys quality, the China National Paints and Pigments Standardization Technical Committee introduced