9431
TLCHPLC
Cd Pb Hg 2 ppm 30 ppm 2 ppm
T.L.C. HPLC mau DAD1 B, Sig=280,4 Ref =550,100 (D:\BASE\09140029.D) 200 150 hesperidin 100 50 0 0 10 20 30 40 50 min
min mau 140 120 100 80 60 40 20 0 DAD1 E, Sig=320,4 Ref =550,100 (C:\LMC\AAHPLC\ \890703.D) AA- I AA- II -20 0 2.5 5 7.5 10 12.5 15 17.5 20 22.5
GMP (Good Manufacturing Practice ) - 1937 Sulfonamides 1938 1962 FDA
GMP () 1963 GMP 1969WHO GMP 1972 GMP 1980 63 GMP
GMP
GMP 1982 GMP 1987 GMP 1999 200531 GMP
B
41,000 (IRB, EC or JIRB)
() (Case Report Form)
() CMC (Investigator brochure)
\\ \ \\\\ \ \
Aflatoxin B1B2G1G2 15 10 0.5 M1 WHO 15 15 0.5 0.05 20 B1 10-20 B1 0.5 M1
( )
90 91 92 B