Protocol 1. 2. 3. 4. / ~ / 1. 2. 3. 1
Genetic modified organisms 1. 2. 3. 4. 5. 6. 7. / 2
/ / Good Laboratory Practice, GLP / / / ~ / 1. 2. 3. 4. 5. 6. 3
1. 2. 3. 4. 5. 4
European Plant Protection Organization, EPPO Food and Agriculture Organization of United Nations, FAO 5
Experiment error Coefficient of variation; CV 6
Environment Protection Agency, USEPA 7
Good Agricultural Practices, GAPs CODEX Alimentarius Commission, CAC 1. 60 mm 2. 60 mm 200 mm 1. 8
2. (1 3 0 (2 3. 4. (1 (2 (3 (4 (5-18 (6 (7 5. (1 a. b. 9
c. (2 a. b. c. ( (3 a. b. c. d. (4 a. b. c. ( d. (5 (6 6. 10
7. 1. -18 (1 (2 (3 ( ( (4 0.5 cm 2 (5 (6 ( 0.5 cm 2 (7 (8 0.5 cm 2 2. 11
(1 a. Calibration curve b. Coefficient of determination R 2 0.995 c. (Limit of Detection, LOD singnal/noise ratio, S/N 3 d. (Limit of Quantification, LOQ S/N 10 e. Method detection limit, MDL MDL = LOQ / 0.1 g/g MDL 1/5 0.1 g/g MDL MRL 1/2 0.025 g/g MDL (2 Blank Recovery 80-120% (3 Recovery 80-120% 0.01 µg/g Relative Standard Deviation RSD 20% (4 Quality Control 80-120% (5 Sample analysis 0.01 12
µg/g RSD 20% (6 Stability of storage -18 80-120% RSD 40% (0.01 µg/g 30% (0.1 µg/g 20% (1 µg/g 80-120% 13
14 ( ( ( ( ( (
15 ( ( (.. l ( (.
. 16
17
18
19