检测报告 (Test Report) 报告编号 (NO.):10102221-014 日期 (Date):2010.10.28 Page 1 of 5 委托单位 Applicant: 江苏迪飞达电子有限公司 JIANGSU DIFEIDA ELECTRONICS CO.,LTD. 委托单位提供样品信息如下 : The following sample(s) was/were submitted and identified on behalf of the client as: 样品名称 Sample Name: 双面板厂内型号 Factory Model: DFD-2-5 组成部分及型号 Component and Model: 板材 (FR-4)/KB-6160 阻焊油墨/PSR-2000LF03HF 字符油墨 /UM-1000EW 镀金药水供应商 Supplier Name: 建滔积层板 ( 昆山 ) 有限公司 太阳油墨 ( 苏州 ) 有限公司 广州宇圣电子材料有限公司 中南电子材料 样品接收日期 Sample Received Date: 2010.10.22 样品检测日期 Test Period: 2010.10.22-2010.10.28 检测方法 : 依照 IEC62321 Edition 1.0:2008 的方法 : 电子电器产品中限用物质含量的测定程序 Test Method: With reference to IEC62321 Edition 1.0:2008 Method: Regulated Substances Content of test process with Electrical & Electronic Products; (1) 用原子吸收光谱仪测定铅的含量 Lead Analysis is performed by AAS (2) 用原子吸收光谱仪测定镉的含量 Cadmium Analysis is performed by AAS (3) 用电感耦合等离子体原子发射光谱仪测定汞的含量 Mercury Analysis is performed by ICP-OES (4) 用紫外 - 可见分光光度计测定六价铬的含量 Hexavalent Chromium Analysis is performed by UV (5) 用气相色谱 - 质谱仪测定多溴联苯和多溴联苯醚的含量 PBBs and PBDEs Analysis is performed by GC-MS 依照 EPA 3540C 的方法, 用液相色谱质谱联用仪测定全氟辛烷磺酸, 全氟辛酸铵的含量 With reference to EPA 3540C method, PFOS,PFOA Analysis is performed by LCMS 检测结果 Test Result: 请参见下页 Please refer to next page(s) 编制人 Edited by: 审核人 Checked by: 批准人 Approved by:
检测报告 (Test Report) 报告编号 (NO.):10102221-014 日期 (Date):2010.10.28 Page 2 of 5 检测结果 Test Result ( 单位 Unit:mg/kg) 检测项目 Test Item 方法检出限 MDL 检测结果 Test Result RoHS 限量 RoHS Limit 铅 (Lead) 1 未检出 (N.D.) 1000 镉 (Cadmium) 1 未检出 (N.D.) 100 汞 (Mercury) 1 未检出 (N.D.) 1000 六价铬 (Hexavalent Chromium) 1 未检出 (N.D.) 1000 多溴联苯 (PBBs) 1000 一溴 (Bromobiphenyl) 5 未检出 (N.D.) 二溴 (Dibromobiphenyl) 5 未检出 (N.D.) 三溴 (Tribromobiphenyl) 5 未检出 (N.D.) 四溴 (Tetrabromobiphenyl) 5 未检出 (N.D.) 五溴 (Pentabromobiphenyl) 5 未检出 (N.D.) 六溴 (Hexabromobiphenyl) 5 未检出 (N.D.) 七溴 (Heptabromobiphenyl) 5 未检出 (N.D.) 八溴 (Octabromobiphenyl) 5 未检出 (N.D.) 九溴 (Nonabromobiphenyl) 5 未检出 (N.D.) 十溴 (Decabromobiphenyl ) 5 未检出 (N.D.) 多溴联苯醚 (PBDEs) 1000 一溴 (Bromodiphenyl ether) 5 未检出 (N.D.) 二溴 (Dibromodiphenyl ether) 5 未检出 (N.D.) 三溴 (Tribromodiphenyl ether) 5 未检出 (N.D.) 四溴 (Tetrabromodiphenyl ether) 5 未检出 (N.D.) 五溴 (Pentabromodiphenyl ether) 5 未检出 (N.D.) 六溴 (Hexabromodiphenyl ether) 5 未检出 (N.D.) 七溴 (Heptabromodiphenyl ether) 5 未检出 (N.D.) 八溴 (Octabromodiphenyl ether) 5 未检出 (N.D.) 九溴 (Nonabromodiphenyl ether) 5 未检出 (N.D.) 十溴 (Decabromodiphenyl ether) 5 未检出 (N.D.)
检测报告 (Test Report) 报告编号 (NO.):10102221-014 日期 (Date):2010.10.28 Page 3 of 5 检测结果 Test Result ( 单位 Unit:mg/kg) 检测项目 Test Item 方法检出限 MDL 检测结果 Test Result 全氟辛烷磺酸 (PFOS) 2 未检出 (N.D.) 全氟辛酸铵 (PFOA) 2 未检出 (N.D.) 备注 Note:(1) mg/kg = ppm (2) = 未规定 Does not stipulate (3) N.D. = 未检出 Not Detected (<MDL) (4) MDL = 方法检出限 Method Detection Limit (5) 最大允许极限值引用 2002/95/EC RoHS 指令和后续修正指令 2005/618/EC The most allowable limit value reference to 2002/95/EC RoHS Directive & its subsequent amendment Directive 2005/618/EC 照片 Photo: 仅对报告照片中的样品负责 Pony authenticate the photo on original report only
检测报告 (Test Report) 报告编号 (NO.):10102221-014 日期 (Date):2010.10.28 Page 4 of 5 检测流程图 Measurement Flow-chart 样品按照下述流程被完全消解 ( 六价铬和多溴联苯 / 多溴联苯醚除外 ) These Samples Were Dissolved Totally By Pre-conditioning Method According To Below Flow Chart. (Cr 6+ And PBBs/PBDEs Test Method Excluded) 预处理 Sample Preparation 称量 Sample Measurement 铅 / 镉 / 汞 Pb/Cd/Hg 多溴联苯 / 多溴联苯醚 PBBs/PBDEs 六价铬 Cr 6+ 微波消解仪 / 电热板酸消解 Acid digestion with microwave/hotplate 过滤 Filtration 溶剂萃取 Sample solvent extraction 浓缩 / 稀释 Concentration/ Dilution 加入萃取液 Adding extraction solution 90-95 条件下萃取 Heating to 90-95 for extraction 溶解 Solution 残渣 Residue 过滤 Filtration 过滤 / 调 ph Filtration and ph adjustment 完全溶解 dissolved totally ashing GC-MS 加入 1,5- 二苯碳酰二肼显色 Adding 1,5- diphenylcarbazide for color development AAS/ICP-OES UV-Vis
检测报告 (Test Report) 报告编号 (NO.):10102221-014 日期 (Date):2010.10.28 Page 5 of 5 PFOS,PFOA Measurement Flow-chart 制样 Sampling 方法适用于均匀材质 Methods for coordination (Which part was sampled like any?) Body 样品称量 Amount of sampling: 1g. 前处理 Pre-conditioning 仪器名称 Instrument name:ultrasontic apparatus 分解用药品名 Medicine name used for decomposition: 甲醇 Methanol 测试 Measurement 测试仪器名称及型号 Measuring instrument name and model:lcms-quattro Premier XE 测试仪器生产商 Measuring instrument manufacturer:ab(usa) 检测器 Detector:MS 测试结果 Measurement result *** 报告结束 End of Report***