CE_2014_53244.xlsm

Transcription

1 號碼 (No.) CE/2014/53244 日期 (Date) 2014/05/26 頁數 (Page) 1 of 8 以下測試樣品係由申請廠商所提供及確認 (The following sample(s) was/were submitted and identified by/on behalf of the applicant as) 送樣廠商 (Sample Submitted By) 樣品名稱 (Sample Description) 收件日期 (Sample Receiving Date) 測試期間 (Testing Period) 2014/05/19 TO 2014/05/26 () ICT PROBE 2014/05/19 =============================================================================================================== 測試需求 (Test Requested) (1) 依據客戶指定, 進行鎘, 鉛, 汞, 六價鉻, 多溴聯苯, 多溴聯苯醚測試. (As specified by client, to test Cadmium, Lead, Mercury, Cr(VI), PBBs, PBDEs contents in the submitted sample.) (2) 依據客戶指定, 進行鹵素 - 氟 氯 溴 碘測試. (As specified by client, to test Halogen-Fluorine, Chlorine, Bromine, Iodine contents in the submitted sample.) 測試方法 (Test Method) 請見下一頁 (Please refer to next pages). 測試結果 (Test Results) 請見下一頁 (Please refer to next pages).

2 號碼 (No.) CE/2014/53244 日期 (Date) 2014/05/26 頁數 (Page) 2 of 8 測試結果 (Test Results) 測試部位 (PART NAME) No.1 金色金屬 ( 含鍍層 ) (GOLDEN COLORED METAL (INCLUDING THE PLATING LAYER)) 鎘 / Cadmium (Cd) 鉛 / Lead (Pb) 汞 / Mercury (Hg) 測試項目 (Test Items) 六價鉻 / Hexavalent Chromium Cr(VI) 鹵素 / Halogen 鹵素 ( 氟 ) / Halogen-Fluorine (F) (CAS No ) 鹵素 ( 氯 ) / Halogen-Chlorine (Cl) (CAS No ) 鹵素 ( 溴 ) / Halogen-Bromine (Br) (CAS No ) 鹵素 ( 碘 ) / Halogen-Iodine (I) (CAS No ) 單位 (Unit) 測試方法 (Method) 參考 IEC 方法, 以感應耦合電漿原子發射光譜儀檢測. / With reference to IEC and performed by ICP-AES. 參考 IEC 方法, 以感應耦合電漿原子發射光譜儀檢測. / With reference to IEC and performed by ICP-AES. 參考 IEC 方法, 以感應耦合電漿原子發射光譜儀檢測. / With reference to IEC and performed by ICP-AES. ** 參考 IEC 方法, 以沸水萃取法方法檢測. / With reference to IEC and performed by Boiling water extraction Method.# 參考 BS EN , 以離子層析儀分析. / With reference to BS EN Analysis was performed by IC. 方法偵測極限值 (MDL) 結果 (Result) No.1 2 n.d n.d. # Negative n.d. 50 n.d. 50 n.d.

3 號碼 (No.) CE/2014/53244 日期 (Date) 2014/05/26 頁數 (Page) 3 of 8 測試項目 (Test Items) 多溴聯苯總和 / Sum of PBBs 一溴聯苯 / Monobromobiphenyl 二溴聯苯 / Dibromobiphenyl 三溴聯苯 / Tribromobiphenyl 四溴聯苯 / Tetrabromobiphenyl 五溴聯苯 / Pentabromobiphenyl 六溴聯苯 / Hexabromobiphenyl 七溴聯苯 / Heptabromobiphenyl 八溴聯苯 / Octabromobiphenyl 九溴聯苯 / Nonabromobiphenyl 十溴聯苯 / Decabromobiphenyl 多溴聯苯醚總和 / Sum of PBDEs 一溴聯苯醚 / Monobromodiphenyl ether 二溴聯苯醚 / Dibromodiphenyl ether 三溴聯苯醚 / Tribromodiphenyl ether 四溴聯苯醚 / Tetrabromodiphenyl ether 五溴聯苯醚 / Pentabromodiphenyl ether 六溴聯苯醚 / Hexabromodiphenyl ether 七溴聯苯醚 / Heptabromodiphenyl ether 八溴聯苯醚 / Octabromodiphenyl ether 九溴聯苯醚 / Nonabromodiphenyl ether 十溴聯苯醚 / Decabromodiphenyl ether 單位 (Unit) 測試方法 (Method) 參考 IEC 方法, 以氣相層析 / 質譜儀檢測. / With reference to IEC and performed by GC/MS. 方法偵測結果極限值 (Result) (MDL) No.1 - n.d. - n.d.

4 號碼 (No.) CE/2014/53244 日期 (Date) 2014/05/26 頁數 (Page) 4 of 8 備註 (Note) = ppm;0.1wt% = 1000ppm n.d. = Not Detected ( 未檢出 ) MDL = Method Detection Limit ( 方法偵測極限值 ) "-" = Not Regulated ( 無規格值 ) **= Qualitative analysis (No Unit) 定性分析 ( 無單位 ) # = a. Positive means the presence of CrVI on the tested areas (Positive 表示測試區域偵測到六價鉻 ) b. Negative means the absence of CrVI on the tested areas (Negative 表示測試區域未偵測到六價鉻 ) The detected concentration in boiling-water-extraction solution is equal or greater than 0.02 with 50 cm² tested areas. / 該溶液濃度 0.02 with 50 cm² (tested areas) 樣品的測試是基於申請人要求混合測試, 報告中的混合測試結果不代表其中個別單一材質的含量. (The samples was/were analyzed on behalf of the applicant as mixing sample in one testing. The above results was/were only given as the informality value.)

5 號碼 (No.) CE/2014/53244 日期 (Date) 2014/05/26 頁數 (Page) 5 of 8 1) 根據以下的流程圖之條件, 樣品已完全溶解 ( 六價鉻測試方法除外 ) / These samples were dissolved totally by pre-conditioning method according to below flow chart.(cr 6+ test method excluded) 2) 測試人員 楊登偉 / Name of the person who made measurement Climbgreat Yang 3) 測試負責人 張啟興 / Name of the person in charge of measurement Troy Chang 剪裁 製備樣品 / Cutting Preparation 測試樣品重量 / Sample Measurement 鉛 Pb 鎘 Cd 依據不同樣品的材質而以適當的酸進行消化 ( 如下表所示 ) / Acid digestion by suitable acid depended on different sample material (as below table) 汞 Hg 硝酸 / 鹽酸 / 氫氟酸的微波消化 / Microwave digestion with HNO 3/HCl/HF 六價鉻 Cr 6+ (Note**) 添加適量消化液 / Add appropriate amount of digestion reagent 溶液 / Solution 過濾 / Filtration 殘渣 / Residue 加熱至適當溫度進行消化萃取 / Heat to appropriate temperature to extract 感應耦合電漿原子發射光譜儀 / ICP-AES 1) 鹼熔融法 / Alkali Fusion 2) 鹽酸溶解 / HCl to dissolve 冷卻後過濾樣品 / Cool, filter digestate through filter 樣品材質 / Sample Material 消化酸液種類 / Digestion Acid 鋼, 銅, 鋁, 焊錫 / Steel, copper, aluminum, solder 王水, 硝酸, 鹽酸, 氫氟酸, 雙氧水 / Aqua regia, HNO 3, HCl, HF, H 2O 2 玻璃 / Glass 硝酸, 氫氟酸 / HNO 3/HF 金, 鉑, 鈀, 陶瓷 / 王水 / Aqua regia Gold, platinum, palladium, ceramic 銀 / Silver 硝酸 / HNO 3 塑膠 / Plastic 硫酸, 雙氧水, 硝酸, 鹽酸 / H 2SO 4, H 2O 2, HNO 3, HCl 其他 / Others 加入適當的試劑至完全溶解 / Added appropriate reagent to total digestion 加入發色劑顯色 / Add diphenyl-carbazide for color development 以紫外光 - 可見光光譜儀, 量測樣品溶液在 540 nm 的吸收度 / measure the absorbance at 540 nm by UV-VIS Note**(1) 針對非金屬材料加入鹼性消化液, 加熱至 90~95 萃取. / For non-metallic material, add alkaline digestion reagent and heat to 90~95. (2) 針對金屬材料加入純水, 加熱至沸騰萃取. / For metallic material, add pure water and heat to boiling.

6 號碼 (No.) CE/2014/53244 日期 (Date) 2014/05/26 頁數 (Page) 6 of 8 多溴聯苯 / 多溴聯苯醚分析流程圖 / PBB/PBDE analytical FLOW CHART 測試人員 翁賜彬 / Name of the person who made measurement Roman Wong 測試負責人 張啟興 / Name of the person in charge of measurement Troy Chang 初次測試程序 / First testing process 選擇性篩檢程序 / Optional screen process 確認程序 / Confirmation process Sample / 樣品 Sample pretreatment / 樣品前處理 Screen analysis / 初篩分析 Sample extraction 樣品萃取 / Soxhlet method 索式萃取法 Concentrate/Dilute Extracted solution 萃取液濃縮 / 稀釋 Filter / 萃取液過濾 Analysis by GC/MS / 氣相層析質譜儀分析 Issue Report 撰打報告

7 號碼 (No.) CE/2014/53244 日期 (Date) 2014/05/26 頁數 (Page) 7 of 8 鹵素分析流程圖 / Analytical flow chart of halogen content 測試人員 陳恩臻 / Name of the person who made measurement Rita Chen 測試負責人 張啟興 / Name of the person in charge of measurement Troy Chang 樣品前處理 / 分樣 / Sample pretreatment/separation 秤重及將樣品放入樣品槽中 / Weighting and putting sample in cell 燃燒彈 / 吸收 Oxygen Bomb Combustion / Absorption 稀釋至固定體積 / Dilution to fixed volume 離子層析儀分析 / Analysis was performed by IC

8 號碼 (No.) CE/2014/53244 日期 (Date) 2014/05/26 頁數 (Page) 8 of 8 #PIC * 照片中如有箭頭標示, 則表示為實際檢測之樣品 / 部位. * (The tested sample / part is marked by an arrow if it's shown on the photo.) ** 報告結尾 (End of Report) **