Microsoft Word 王超-二校出三页

Size: px

Start display at page:

Download "Microsoft Word 王超-二校出三页"

溥牧郭
7 years ago
Views:

1 6 1 Vol. 6 No Journal of Food Safety and Quality Jan., 2015 B 2 王超 1, 赵晶 1*, 余宁江 2 (1., ; 2., ) 摘要 : 目的 B 2 方法, ph B 2 结果 B 2, 1 h 40%; Mg 2+ 5 h B 2 10% ; Fe 3+ Cu 2+ B 2 B 2 ; C 5 h B % ; B 2 ; B 2, 20% 结论 B 2,, C B 2 关键词 : B 2 ; ; Study on stability factors of vitamin B 2 in infant food additives WANG Chao 1, ZHAO Jing 1*, YU Ning-Jiang 2 (1. Department of Food and Environment Engineering, East University of Heilongjiang, Harbin China; 2. Wondersun Dairy Company of Heilongjiang, Harbin , China) ABSTRACT: Objective To study the impact factors of vitamin B 2 stability in infant formula powder. Methods Illumination, temperature, ph, metal ions, oxidants, antioxidants, preservatives and sugar were studied on the stability of vitamin B 2 by UV visible spectrophotometry. Results Effect of light on vitamin B 2 was the biggest, with its 1-h loss rate of 40%; Mg 2+ could cause vitamin B 2 loss rate to 10% after 5 h, Fe 3 + and Cu 2 + could cause damage through react with vitamin B 2 and generate other substances; Vitamin C could cause about 13.8% loss of vitamin B 2 ; Common food additives, such as potassium sorbate, sodium benzoate, and oxidant hydrogen peroxide had the limited effect on vitamin B 2 ; Glucose could not cause the loss of vitamin B 2, and sugar could cause the loss of 20%. Conclusion The stability of vitamin B 2 is affected by many factors, among which the greatest impact is the light; some metal ions, vitamin C and sucrose also affect the stability of vitamin B 2. KEY WORDS: vitamin B 2 ; stability; infant food additives 1 引言 B 2,, [1] ( ), B 2,, B 2, B 2,, B 2 * 通讯作者 :,, [email protected] *Corresponding author: ZHAO Jing, Associate Professor, Department of Food and Environment Engineering, East University of Heilongjiang, No.331, Xuefu Road, Nangang District, Harbin , China. [email protected]

2 1, : B : - [2, 3] [4],, B 2 [5], B 2, B 2,, B 2,, B 2, 1 B 2 Fig. 1 UV absorption curve of vitamin B 2 2 材料与方法 2.1 仪器与试剂 (DHP-9012 ) (SP-752 ) (HWS-26 ) ph (S20 - ) (JJ200 ) B 2 ( )( ) C ( )( ) A ( )( ) ( )( ) ( ) ( )( ) ( )( ) ( ) ( ) 2.2 实验方法维生素 B 2 标准液配制 B 2 5 mg( g), 500 ml, 10 μg/ml B 2 [7] 维生素 B 2 标准曲线的绘制 B 2 B 2 200~500 nm [6], 1 B nm, B 2, B 2 [11] 2 B 2 2 B 2 Fig. 2 Standard curve of vitamin B 探究光照对维生素 B 2 稳定性的影响 B 2, 15, 20 ml B 2, 5, 5, 5,, 1 h, 探究温度对维生素 B 2 稳定性的影响 B 2, 20, 20 ml B 2,, ( ), 1 h, 探究 ph 值对维生素 B 2 稳定性的影响 ph ph ml 25, 20 ml B 2,,, 1 h 探究金属离子防腐剂氧化剂抗氧化剂及糖类对维生素 B 2 稳定性的影响, B 2, 20 ml B 2,, (Na + K + Ca 2+ Fe 3+ Cu 2 ) (

3 286 6 ) (H 2 O 2 ) (Vc) ( ), 5 h, 1 h, 5, B 2 B 2 3 结果与分析 3.1 光照对维生素 B 2 的影响 3, 1 h B 2 59%, B 2, B 2, 5 h 95%, B 2, 6.7% [12],, [7] 4 B 2 Fig. 4 Effects of temperature on stability of vitamin B 2 5 ph B 2 Fig. 5 Effects of ph value on stability of vitamin B 金属离子对维生素 B 2 的影响 3 B 2 6, B 2 Na + B 2, K + Ca 2+ B 2 3%-5% ; Mg 2+ B 2, 10%; Fe 3+ Cu 2+ B 2 [8] Fig. 3 Effects of light influence on stability of vitamin B 温度对维生素 B 2 的影响 4, B 2, 5 h 8%, 25 5 h 6%, 40 60, B 2, B ph 对维生素 B 2 的影响 5, B 2, 5 h 94% 96.4%,, 77.9%, ph, B 2 6 B 2 Fig. 6 Effects of metal ions on stability of vitamin B 氧化剂及抗氧化剂对维生素 B 2 的影响 7, B 2, C [13] B 2, 5 h B %

4 1, : B 结论 7 B 2 Fig. 7 The oxidant and antioxidant influence on vitamin B 2 stability 3.6 防腐剂对维生素 B 2 的影响 8, B 2 B 2, B 2,, B 2 [14] [9] [10] B 2 B 2, B 2 Mg 2+ 5 h B 2 10%, Fe 2+ Cu 2+ B 2, B 2,, 20%, C B 2, C B 2 参考文献 [1],,,. B 2 [J]., 2010, 27(2): Liu W, Wang H, Zhu CS, et al. Fluorescence spectrophotometry determination of vitamin B 2 in the urine [J]. Trace Elements Health Res, 2010, 27(2): B 2 Fig. 8 Preservative influence on vitamin B 2 stability 3.7 糖类对维生素 B 2 的影响 9, B 2, 20% B 2, B % 9 B 2 Fig. 9 Effects of glucose and sucrose on stability of vitamin B 2 [2],,,. B 2 [J]., 2012, 12(2): 4 6. Lv GB, Liu FQ, Li XZ, et al. Ultraviolet spectrophotometry uncertainty analysis of content of vitamin B 2 injection [J]. Cap Med, 2012, 12(2): 4 6. [3],,, [J]., 2007, 17(7): Wang YH, Feng JL, Pan ZQ et al. Liquid chromatography - tandem mass spectrometry analysis of 10 kinds of water-soluble vitamins [J]. Chin J Health Inspect, 2007, 17(7): [4] GB B 2 [S]. GB The determination of vitamin B 2 in infant food and milk products [S]. [5],,,. B 2 [J]., 2013, 41(2): Guan YY, Lin HD, Zou ZF. et al. Infant formula in the rapid determination of vitamin B 2 [J]. China Dairy Ind, 2013, 41(2): [6]. [D]. :, 2010, Fan TT. Study on Vitamin of fluorescence spectrum and analysis

288 6 method [D]. Shijiazhuang: Hebei Normal University, 2010, 10 12. [7] 垚. D [D]. :, 2013, 23 30. Fan Y. The study of stability of vitamin D in babies and infants powdered formula [D].

Non-destructive Detection of Vitamin B 2 in Plant Leaves Using Fluorescence Monitoring[J]. Shokubutsu Kankyo Kogaku, 2011, 23 (4): 152 158. [9],,,. [J]., 2010, 38(30): 16845 16725.

5 288 6 method [D]. Shijiazhuang: Hebei Normal University, 2010, [7] 垚. D [D]. :, 2013, Fan Y. The study of stability of vitamin D in babies and infants powdered formula [D]. Changsha: Central South Forestry University of Science and Technology, 2013, [8] Kazuya SS, Kentaro YG, Kenzo Y. et al. Non-destructive Detection of Vitamin B 2 in Plant Leaves Using Fluorescence Monitoring[J]. Shokubutsu Kankyo Kogaku, 2011, 23 (4): [9],,,. [J]., 2010, 38(30): Wang SW, Gong J, Gao A, et al. The research on preservative sodium benzoate of pharmacology and toxicology [J]. Anhui Agric Sci, 2010, 38(30): [10],,,. [J]., 2010, 22(3): Int J Food Sci Nutr, 2011, 62(3): [13]. C [D]. :, Liu YB. The study of stability of vitamin C in infant formula powder [D]. Changshan: Central South Forestry University of Science and Technology, [14]. [J]., 2011, 11: Wang GJ. The performance and application of potassium sorbate [J]. China Food, 2011, 11: [15],. VE [J]., 2012, 24(19): 83. Mao CD, Mao WZ. The metal cation study of VE acetate decomposition [J]. Ind Technol, 2012, 24(19): 83. ( 责任编辑 : 白洪健 ) 作者简介 Zhang Q, Ying CY, Yu KN, et al. Hydrogen peroxide decomposition rate and stability study [J]. J Jiaxing Coll, 2010, 22(3): [11],,,. 王超, 硕士研究生, 主要研究方向为食品添加剂 [email protected] [J]., 2001, 29(5): Pan JG, Wang KF, Zhang YL, et al. High performance liquid chromatography (HPLC) method to simultaneous determination of water-soluble vitamins in pollen [J]. J Tongji univ, 2001, 29(5): 赵晶, 副教授, 主要研究方向为食品加工技术 [email protected] [12] Rodrigues MR, Paulo H, Lacerda FV. Use of chitosan in the treatment of obesity; evaluation of interaction with vitamin B 2 [J].

mm ~

mm ~ 16 3 2011 6 Vol 16 No 3 JOURNAL OF HARBIN UNIVERSITY OF SCIENCE AND TECHNOLOGY Jun 2011 1 2 3 1 150040 2 150040 3 450052 1 3 4 > 1 ~ 3 > > U414 A 1007-2683 2011 03-0121- 06 Shrinkage Characteristics of

Microsoft Word 王超-二校 出 三页

Microsoft Word 王超-二校出三页