C 52 GBZ GBZ/T 160.30 2004 Methods for determination of inorganic phosphorus compounds in the air of workplace 2004 5 21 2004 12 1
GBZ/T 160.30-2004 GBZ 1 GBZ 2 [ Phosphorus pentoxide Phosphorus pentasulfide Yellow phosphorus Phosphine Phosphorus trichloride Phosphorus thiochloride Phosphorus oxychloride ] 2004 12 1 GB/T16037 1995 GB/T16036 1995 GB11516 89 GB/T 16110 1995 1989
GBZ/T 160.30 2004 1 2 GBZ 159 3 3.1 680nm 3.2 3.2.1 0.8µm 3.2.2 40mm 3.2.3 25mm 3.2.4 0 3L/min 0 10L/min 3.2.5 10ml 3.2.6 50ml 3.2.7 100ml 3.2.8 3.2.9 3.3 3.3.1 20 1.84g/ml 3.3.2, 10mol/14.4ml 100ml 3.3.3 15g/ 3.3.4 50g/ 3.3.5 0.1389g KH 2 PO 4 100ml 1.0mg/ml 10.0µg/ml 3.4 GBZ 159 3.4.1 5L/min 15min 3.4.2 1L/min 4 8h 3.4.3 1L/min 2 8h 2 3d
3.5 3.5.1 3.5.2 10ml 10min 50ml 20ml 3.5.3 6 0.0 0.25 0.50 1.0 1.50 2.0 ml 10ml 0.0 2.5 5.0 10.0 15.0 20.0µg 0.5ml 5ml 2ml 50ml 10min 680nm 3 µg 3.5.4 (µg) 3.6 3.6.1 1 293 P Vo = V 1 273 + t 101.3 Vo V t P kpa 3.6.2 2 m C = 2 Vo C mg/m 3 m µg Vo 3.6.3 GBZ 159 3.7 3.7.1 0.4µg/ml 0.26mg/m 3 75 2.6 6.4 3.7.2 99 3.7.3 3.7.4 4 4.1 GDX 101 4.2 4.2.1 1.5 4.2.2 4.2.3 1000ml 4.2.4 1 2 5 50 100ml
4.2.5 526nm 1m 4mm GDX 101 100 150 150 4.3 4.3.1 4.3.2 GDX 101 40 60 4.3.3 20 (V/V) 4.3.4 2 50ml 4.3.4.1 0.1mol/ 1mol/ 4.3.4.2 5mol/28.8ml 100ml 4.3.4.3 4.3.4.4 2.5g 100ml 1 4.3.4.5 50g/ 4.3.4.6 0.4002g KH 2 PO 4 100ml 1.0mg/ml 5.0 g/ml 4.3.4.7 6 0.00 0.20 0.40 0.60 0.80 1.00ml 2.0ml 0.0 1.0 2.0 3.0 4.0 5.0µg 2 5ml 0.3ml 0.2ml 1 50 10min 680nm µg 4.3.4.8 10000 100ml 2.0ml 3 m C = f 3 v C mg/ m µg v ml f 4.4 GBZ 159 5 6 7d 4.5 4.5.1 4.5.2 4.5.3 4 100ml 0.010 0.050 0.20
1.0ng/ml 1.0ml 3 µg 4.5.4 (µg) 4.6 4 m C = (4) V C mg/ m 3 m ng V ml 4.7 4.7.1 0.001mg/m 3 1ml 0.001 1mg/m 3 4.0 9.1 4.7.2 100ml 2h 15d 5 5.1 680nm 5.2 5.2.1 5.2.2 0 3L/min 5.2.3 10ml 5.2.4 5.2.5 5.3 5.3.1 20 1.84g/ml 5.3.2 0.1mol/ 1mol/ 5.3.3 5mol/28.8ml 100ml 5.3.4 5.3.5 2.5g 100ml 1 5.5.6 50g/ 5.3.7 0.4002g KH 2 PO 4 100ml 1.0mg/ml 5.0 g/ml 5.4 GBZ 159 10.0ml 1L/min 15min 5.5 5.5.1 10.0ml
5.5.2 3 2.0ml 5.5.3 6 0.00 0.10 0.20 0.30 0.50 0.70ml 2.0ml 0.00 0.50 1.00 1.50 2.50 3.50µg 2 5ml 0.3ml 0.2ml 1 50 10min 680nm 3 µg 5.5.4 (µg) 5.6 5.6.1 1 5.6.2 5 5 m C = 5 Vo C mg/m 3 m µg Vo 5.7 5.7.1 0.1µg/ml 0.07mg/m 3 15 0.1 1.75µg/ml 2.8 8.5 5.7.2 92 100 5.7.3 0.80 0.95mol/ 5.7.4 6 6.1 680nm 6.2 6.2.1 6.2.2 0 3L/min 6.2.3 10ml 6.2.4 6.2.5 6.3 6.3.1 20 1.84g/ml 6.3.2 15g/ 6.3.3 5mol/28.8ml 100ml 6.3.4
6.3.5 6.3.6 2.5g 100ml 1 6.3.7 50g/ 6.3.8 6.3.8.1 0.2454g K 2 HPO 4 1000ml 100µg/ml 10.0µ g/ml 6.3.8.2 0.1389g KH 2 PO 4 1000ml 100µg/ml 10.0µg/ml 6.4 GBZ 159 10.0ml 400ml/min 15min 1L/min 15min 6.5 6.5.1 10.0ml 6.5.2 6.5.2.1 3 15min 5.0ml 6.5.2.2 3 10ml 5.0ml 6.5.3 6.5.3.1 6 0.00 0.20 0.40 0.60 0.80 1.00ml 5.0ml 0.0 2.0 4.0 6.0 8.0 10.0µg 0.5ml 0.2ml, 1 10min 680nm 3 µg 6.5.3.2 16 0.00 0.25 0.50 1.00 2.00 3.00 4.00 5.00ml 5.0ml 0.0 2.5 5.0 10.0 20.0 30.0 40.0 50.0µg 0.5ml 1min 1 0.5ml 0.2ml, 1 10ml 10min 680nm 3 µg 6.5.4 (µg) 6.6 6.6.1 1 6.6.2 6 2 m C = 6 Vo C mg/ m 3
m g Vo 6.6.3 7 2 m C = 1.4 7 Vo C mg/ m 3 1.4 m g Vo 6.6.4 GBZ 159 6.7 6.7.1 0.2µg/ml 0.5µg/ml 0.26mg/ m 3 7.5L 0.5mg/ m 3 6 0.2 2µg/ml 0.5 10µg/ml 9.7 4.2 6.7.2 89 100 93 100 6.7.3 0.80 0.95mol/ 6.7.4 7 7.1 665nm 7.2 7.2.1 7.2.2 0 3L/min 7.2.3 10ml 7.2.4 7.2.5 7.3 7.3.1 20 1.84g/ml 7.3.2 A 15ml 4g 4g EDTA 1g 1 7.3.3 B 0.5g 10ml 1 7.3.4 A 217ml 500ml 1 7.3.5 B 50ml 30ml 7.3.6 12g B 1 7.3.7 90g/ 7.3.8 0.25ml A 10ml 2ml
7.3.9 7.3.9.1 0.1212g 23 A 100ml 1 mg/ml A 10µg/ml 7.3.9.2 25ml 10ml 2 3 40.0 g/ml 7.4 GBZ 159 10.0ml 0.5L/min 15min 2 7.5 7.5.1 10.0ml 7.5.2 3 10.0ml 4.0ml A B 1ml 1ml 7.5.3 7.5.3.1 7 0.00 0.05 0.10 0.30 0.50 1.00 1.50ml 5.0ml 0.0 0.10 0.20 0.60 1.0 2.0 3.0 g/ml 0.5ml 50 15min 10min 665nm 3 µg/ml 7.5.3.2 7 0.00 0.10 0.20 0.50 0.60 0.80 1.00ml 1.0ml 4.0ml B 0.0 0.80 1.60 3.20 4.80 6.40 8.00µg/ml 60 50min 0.5ml 665nm 3 µg/ml 7.5.4 A B µg/ml 7.6 7.6.1 1 7.6.2 8 10 c A c B C 8 Vo C mg/ m 3 10 ml c A c B A B µg/ml Vo 7.6.3 GBZ 159 7.7 7.7.1 0.2µg/ml 0.93µg/ml 0.3mg/m 3 1.2mg/m 3 7.5 0.2 3.0µg/ml
0.93 8.0µg/ml 2.1 5.5 3.6 7.5 7.7.2 96 98.7 7.7.3 0.8 g/ml A B 8 8.1 SE-30 QF-1 8.2 8.2.1 8.2.2 0 3L/min 8.2.3 10ml 8.2.4 1µl 10µl 8.2.5 526nm 1.5m 3mm SE-30:QF-1:Chromosorb WAW DMCS = 3:2:100 70 190 200 30ml/min 8.3 8.3.1 100ml 150ml 8.3.2 SE-30 QF-1 8.3.3 Chromosorb WAW DMCS 60 80 8.3.4 25ml 10ml 1.0 g/ml 8.4 GBZ 159 5.0ml 0.5L/min 15min 8.5 8.5.1 5.0ml 8.5.2 3 5.0ml 8.5.3 0.00 0.05 0.10 0.20 0.30 0.50 g/ml 5.0µl 3 g/ml 8.5.4 g/ml 8.6 8.6.1 1
8.6.2 9 5 c C 9 Vo C mg/ m 3 5 ml c µg/ml Vo 8.6.3 GBZ 159 8.7 8.7.1 0.04µg/ml 0.03mg/m 3 7.5 0.04 0.50µg/ml 8.2 8.7.2 93 8.7.3 8.7.4