犐犆犛 27.010 犉 01 犜犺犲犿犻狀犻犿狌犿犪犾狅狑犪犫犾犲狏犪犾狌犲狊狅犳狋犺犲犲狀犲狉犵狔, 狑犪狋犲狉犮狅狀狊狌犿狆狋犻狅狀犪狀犱犵狉犪犱犲狊犳狅狉犱犻狊犺狑犪狊犺犲狉狊! "#$
GB/T1.1 2009!"#$%&' : ()*+,-./01 (23)/01 4 56789:,; /01 <=/01 5>?@AB /01 CD E /01 F(CD)/01 GHIJKL/01 MNOG ( )/01 ()*+ PKL F/01 Q2RISIT UKL VW:< X /01 Q2Y8 /01 U VW Z<X K/01 [\ ]:^_` abc * 2 Ⅰ
1 B B,-.(,-.)P 0 0 P P S B B /,-. B B B,-. 2!"#$ B A B, A B A B, ( / ) B GB/T4214.3 B B J,-. \ GB/T20290 2016 B,-. P S QB/T1520 2013 B B,-. 3 %&' GB/T20290 2016 QB/T1520 2013 L B 3.1 狑犪狊犺犻狀犵犮狔犮犾犲 J,-. = P(,;, ),^ B(),- 3.2 () 犲狀犲狉犵狔犮狅狀狊狌犿狆狋犻狅狀狆犲狉狑犪狊犺犻狀犵犮狔犮犾犲,,-.^! "# $ %,,;B "# P% 3.3 ") 狑犪狋犲狉犮狅狀狊狌犿狆狋犻狅狀狆犲狉狑犪狊犺犻狀犵犮狔犮犾犲,,-.^! B % 3.4 狋犺犲犿犻狀犻犿狌犿犪犾狅狑犪犫犾犲狏犪犾狌犲狅犳狋犺犲犲狀犲狉犵狔犮狅狀狊狌犿狆狋犻狅狀犳狅狉犱犻狊犺狑犪狊犺犲狉狊,,-.^! &'P 3.5 狋犺犲犿犻狀犻犿狌犿犪犾狅狑犪犫犾犲狏犪犾狌犲狅犳狋犺犲狑犪狋犲狉犮狅狀狊狌犿狆狋犻狅狀犳狅狉犱犻狊犺狑犪狊犺犲狉狊,,-.^! &' 4 ' 4.1,-.P 5, 1 P (,-.)JP 1
*+,-.P,, )JP *+ -./ 1 *1 +,-. P EEI WEI 犘 D /db(a) *+ 犘 c 1 50 45 1.08 46 2 56 52 1.08 46 3 63 62 0.97 52 1.12 4 71 68 0.97 52 5 80 75 0.86 58 /:01/ B,-. 4.2,-. 5, 1 (,-.)J P *+,-.,, )J P *+ -./ 2 *2 +,-. WEI P EEI 犘 D /db(a) *+ 犘 c 1 45 50 1.08 46 2 52 56 1.08 46 3 62 63 0.97 52 1.12 4 68 71 0.97 52 5 75 80 0.86 58 /:01/ B,-. 5 0%-. 5.1,-.P *+ 1P 5 5.2 1 62 S,,-.! # %! B % *+ )J 34 56 3 56 2
*3 1 78 56! # % +10%! B % +10% *+ -10% -19% +3dB 6 234 6.1 25$'6 78 GB/T20290 20169: ;, B,; B,J (23±2) 9 < (55±5)% SB = B(2.5±0.5)mmol/L /: = B9>?@, B = A0 ; J 6.2 +9 +9 :;+9' +96 34 6.2.1, <=>?@<=34 BCD E=BC A 6.2.2,?@ E= B B F G@HIE= 6.2.3 GB/T20290 2016 M,-. B, E=JK LM C B F G@HI,-.,N I E=JKN ; JK,-., O P 3.55±0.20, P 0.81±0.10, J 6.2.4?@AB34 %PQR; ST 6.2.5?@CDE AB34 E=BCUV LM D E= WX ST E 6.2.6 J,-.! ; S 3
6.2.7 6 34 Y A N, GB/T20290 20169:J ; 6.2.8 +9 +9 34 P QB/T1520 20139: ; # % # %1 : a) Z [% 狆狊 6\,-., # % # %1 QB/T1520 2013 9: ; b) Z [% 狆狊 <6\,-., # % (1),# % (2) 犛犃犈 c=11.5 狆狊 +230 (1) 犛犠犆 =1.6 狆狊 +11 (2) : 犛犃犈 c 犛犠犆 狆狊 QB/T1520 2013 6.2.9 :;+9' +9 34 *+ ] F ] G *+ QB/T1520 20139: ; 6.3 6 34 GB/T4214.3;, J BE= B 4
犃 ( ) <=>?@<=34 犃.1 <=> BCD7 BCE= ^_; `a; bc; ; ; ; D 犃.2 <=> F8'G" 犃.2.1 H"-. Y /, S B /BCD % S \ BCD %(g/\ \ ), &B E= ^_BCD B B `abcd `a (1h) BCD `a,: X, 10min BC^ /E=K1 X,, 80 2h( BC Y ) 犃.2.2 IJ GB/T20290 2016 6.4.1; 犃.2.3 KL GB/T20290 2016 6.4.2; BWX ;, E N, $BC; ` B% 120mL 犃.2.4 MN 犃.2.4.1 F8'O Y [,bc GB/T20290 2016 6.4.3.1; %b^c b c1 1 - b c B 4.5mm( 50 ) b. c c 700g( 150r/min) bc, H B X 犃.2.4.2 G" BCE= BCB% BC : 5
a) BCE= 1/2 % - 1/2 % - b) BCB% -3g/ 2g/ -4g/ 1g/ c) BC B, E= %, BCD, %bc 犃.2.5 犃.2.5.1 F8 K1[, %[ bc B BCD- /E=A, /B % [ bc % BCD % BCD, H % 7 BC: BC - -: bcbcd - - $, 20mm *+ - %, %, - bc( B ) bc( B ),,9 BC DB% 50% BC : bc B%1g B bc / A,, AK B A, % 50g~65g K7d, / X, B K B1 &,B - -, 犃.2.5.2 G" BCE= BCB% BC : a) BCE= 1/2 % - 1/2 % - 1/2 % b) BCB% -1g/ -1.5g/ 1/4,0.05g/ 0.5g/ 1g/ c) BC B!25mm "#, $ \ ]E= % BCD, 6 % K1[, %[ B - % / E=A, /[ M % BCD % BCD, H B% 7 BC: BC : BCD $, 10mm *+ BC - - : BCD /- $, 20mm *+ - %, - ( B &) - %
, - ( Bbc) %, ( B ),, 9 B C D B % 50% BC : BCD- ' $ 1/4 JKMMA.1 犃.2.6 RST 犃.2.6.1 F8 犃.1 PQ B b GB/T20290 2016 E 50g 3 GB/T20290 2016 5.6.3\ 750mL 250mL ^_ % - D / #,B (( )UV) 10min ^ &, B* +,- /: B.=. /0,1 P,. 160mm 犃.2.6.2 G" BCE= BCB% BC : a) BCE= 1/2 % - 1/2 % b) BCB% -2g/ c) BC 7 BC: BC -: B! 25mm "# &- / -, $ &-, 20mm *+ - %, &( B ),,9 BCDB% 50% BC : -! &K S T, 2 3A & 4C,& 5GUV - %, & 2 3A & 4C,& 5GUV BC 7
犃.2.7 UV 犃.2.7.1 F8'O B 67, 8^ 9, B:; GB/T20290 2016 6.4.6.1; 犃.2.7.2 G" BCE= BCB% BC : a) BCE= 1/2 % 1/2 % b) BCB% 5g/ 5g/ 6g/ c) BC B! 25mm "# E= %, BCD \% % K1[, %M B - % /E=A,[ % BCD %,BCD, H B% 7 BC: BC : - / A,& 20mm *+ %, 50% BC : A.2.8.2 犃.2.8 W>XY 犃.2.8.1 F8'O ( B ) %, ( B b c),, 9 B C D B % B D $ <% 75%~85%,& A.1\ * 犃.1 XY )-. <% = (33±10)% > = (33±10)%? = (33±10)% D K X, / B B D \K @ 犃.2.8.2 G" BCE= BCB% BC : a) BCE= 8
1/2 % b) BCB% 1g 1g/ c) BC BC : BC : B D A.2.7.1 1 6 - \ % D / K [, %[ D / % B 7g D / D- % / A, 20mm *+ [ D / M % BCD % BCD, H B% BC : B! 25mm "# %, BCD \% 犃.3 <=> 1 %] K1[, %M B ] - % / A, \ -,[ ] % BCD %,BCD, H B% K1WX 犃.3.1 6Z 6Z[\ 6\ 6\ A,-.BCD %N ( 12\E= ), A.2 * 犃.2 6Z 6Z[\ <=>9) 1 BC TE= ^_ bc & `a D -(12) 1g 6 2g 6 -(6) 3g 3 1.5g 3 (24) 1/4 (6) 0.5g 6 (12) 41 6 1g 6 (6) 1g 3 5g 3 (6) 2g 3 5g 3 -(1) 4g (1) 6g 1g (1) (1) AB (6) (6) /: 10mL 6 1g 41 120mL 6 9
犃.3.2 6Z[] 6\,-.BCD %N ( 4\E= ), A.3 * 犃.3 6Z[] <=>9) 1 BC TE= ^_ bc & `a D -(4) 1g 2 2g 2 -(3) 3g 1 1.5g 1/2 0.75g 1/2 1.5g 1 (8) 1/4 (2) 0.5g 2 (4) 41 2 1g 2 (2) 1g 1 5g 1 (3) 2g 1 5g 1 1g 1/2 2.5g 1/2 (1) (1) AB (2) (2) /: 10mL 2 1g 41 120mL 2 10
E=> % B.1 犅 ( )?@^9) * 犅.1?@^9) C D E=E /mm %/g 1 2 3 4 5 6 7 8 9 10 11 12 13 ] E= 1H E= 6\ 6\ A % - 117 53 160.0±20.0 \ 1 \ 1-156 58 360.0±25.0 AB 60 120 AB 106 85 94 255.0±20.0 \:\ 0.5-0.5 \:\ 0.5 \:\ 0.5+ 0.5 \:\ 0.5 \:\ 0.5-0.5 \:\ 0.5 230 FG (15.0±3.0)/ \ 2 \ 2 135 40.0±8.0 \ 1 \ 1 208 38 530.0±35.0 \:\ 0.5-0.5 \:\ 0.5 208 28 450.0±30.0 96 23 90.0±10.0 \:\ 0.5+ 0.5 \:\ 0.5 \:\ 0.5+ 0.5 \:\ 0.5-202 98 810.0±50.0 1 0 320 214 34 670.0±40.0 1 0 200 75 I B 1 1 217 63 95.0±10.0 1 1 /:GB/T3532 J?@9:\ B E= 6\ % \:\ 0.5-0.5+1 \:\ 0.5+ 1 \:\ 0.5+ 0.5 \:\ 0.5 \:\ 0.5-0.5 \:\ 0.5 \:\ 0.5-0.5 \:\ 0.5 \:\ 0.5+ 0.5+1 \:\ 0.5+ 1 \:\ 0.5+ 0.5 \:\ 0.5 11
犆 ( ),?@PQ _,-.E=JK LM, MC.1 MC.2 MC.3 /1: KKL K /2:' M, 1~6 BC &, 7~12 BC 犆.1 \`apq _ /: -JK' 3, BCD, &BCDN,OK, &BCD -K 犆.2 `apq _ 12
/1: -JK' 3,', M JK - /2: JK' 3, BCD, BCDN,OK /3: K -, -N M /4: JK' 3, BCD,bcBCDN,OK 犆.3 ]`apq _ 13
犇 ( ) <=><=bc _ 犇.1 IJ ^_BCUV MD.1 MD.2 犇.1 IJ<=bc( ) 犇.2 IJ<=bc( ) 犇.2 KL `abcuv MD.3 14 犇.3 KL<=bc
犇.3 MN bc - -BCUV MD.4~MD.7 犇.4 MNC 犇.5 MNC 犇.6 MNC 犇.7 MNC 15
犇.4 - - BCUV MD.8~MD.12 犇.8 C 犇.9 C 犇.10 C 16 犇.11 C
犇.5 RST 犇.12 C - BCUV MD.13 MD.14 MD.15 犇.13 RSTC 犇.14 RSTC 犇.15 RSTC 17
犇.6 UV BCUV MD.16 MD.17 MD.18 犇.16 UVC 犇.17 UVC 犇.7 W>XY 犇.18 UVC D BCUV MD.19 MD.20 18
犇.19 W>XYC 犇.20 W>XYC 19
犈 ( )?@CDE AB34 犈.1 WX K28\E= /:28\ B.1 E= % 16\ 12\P 犈.2 E=ST ME.1 犈.1?@ AB 犈.3 10 ST ME.2 犈.2 1 AB 犈.4 20 ST ME.3 20
犈.3 2 AB 犈.5 30 -ST ME.4 犈.4 3 AB 犈.6 40 -ST ME.5 犈.5 4 AB 犈.7 50 ST ME.6 犈.6 5 AB 21
犈.8 60AB -ST ME.7 犈.7 6 AB 犈.9 70 ST ME.8 犈.8 7 AB 犈.10 80 ST ME.9 犈.9 8 AB 22
*+ ] F.1 犉 ( ) :;+9 * * 犉.1 :;+9 * C *+E= E= 1-2 - 3 AB 4 5 6 7 8 9 10-11 12 13 F 犫 E= 犪犫 5 4 3 2 1 0 犆 z = 5 犫 =0 犪犫 犫 23
] G.1 犌 ( ) +9 * * 犌.1 +9 * C E= Q R S E= F 犮 E= 犪犮 2 1 0 犇 z = 2 犮 =0 犔犪犮 犮 1-2 - 3 AB 4 5 6 7 8 9 10-11 12 13 24