1 1 2 B 1 2.1 1 2.2 2 2.3 3 3 7 3.1 7 3.2 7 4 9
1 GC HPLC GC HPLC 2 B B B 2.1 B 1 B 2 B 6 B 3 B 5 B 3 B 5 PP B 3 B 5 7 B 7-1 -
B 2 B 1 B 3 B 5 B 3 B 5 (B 3,B 5,PP) (B 6 ) B 2 M H C BT B 12 P 1 2.2 B 2 3 210nm 250-300nm 270nm 210nm 1-2 -
(Abs) (Abs) 2 B 3 B 1 UV (nm) 198 244 223 266 220 264 195 288 196 194 208 260 194 208 260 2.3 LC-10ATvp CTO-10Avp SPD-10Avp C-R6A Shim-pack CLC-ODS( 6.00mm 150mm) SOS - 3 -
2.3.1 B C M PT H 1 B 12 8 2mM SOS 0.8mM 100mM 2 4 5 210nm,270nm 2 Shim-pack CLC-ODS ( 6.0mm 150mm) 100mM (ph2.1) 40 +0.8mM SOS*/ =9/1 1.5mL/min 210nm 270nm * SOS - 4 -
4 (210nm) 5 (270nm) 2.3.2 3 2 3 B - 5 -
2.3.3 6 7 8 6 (210nm) 7 (270nm) ( 10-6) (ng 10-3 ), (ng 10-4 ) 8-6 -
3 Br B 12 P C 3.1 1 CLC-NH 2 2 N + 3 1/1000-1/3000 278nm 550nm 4 3.2 9 4 10~15 4 UV 210 278 196 (nm) 205 213 280 208 200 225 285 190 245-7 -
9 10 8 Shim-pack CLC-ODS(6.0mm15cm) 10mM (ph2.6)+0.2m 40 1mL/min 210nm 11 12 ( Br) - 8 -
Shim-pack CLC-ODS(6.0mm 15cm) 100mM (ph2.1)3 1 40 1.5mL/min 265nm 13 P Shim-pack CLC-NH 2 (6.0mm 15cm) 10mM (ph2.6)/1/3 40 1.5mL/min 245nm 12 14 C 15 4 HPLC - 9 -
ISO ( ) ( ) ( ) 25 INSTEC 5 100029 (010) 6204-3957/3958 (010) 6204-3968 25 INSTEC 5 100029 (010) 6204-3961 (010) 6204-3968 25 INSTEC 5 100029 (010) 6204-3965 (010) 6204-3968 ( ) 755 10 DEF 200020 (021) 6466-4662 (021) 6472-8648 ( ) 97 1 405 110001 (024) 2383-6735 (024) 2383-6378 http://www.shimadzu.com.cn 77 6 F 610015 (028) 8619-8421/8422 (028) 8619-8420 ( 89 27 D2 210029 (025) 471-6502 (025) 470-1704 ) ( ) 604 510015 (020) 8666-9044 (020) 8667-8076 ( 68 18 1806 400010 (023) 6380-6057 6380-6058 (023) 6380-6551 ) ( ) 2F-B 5 710075 (029) 838-6016 (029) 838-6497 ( Suite 1028. Ocean Centre, Harbour City. Tsim Sha tsui, Kowloon, Hong-Kong (00852) 2375-4979 (00852) 2199-7438 ) 26 A 802 830000 (0991) 589-0271 598-0272 (0991) 589-0273 ( 1-3 81(3) 3219-5700( ) 81(3) 3219-5710 ) 432 908 650021 (0871) 315-2987 (0871) 315-2991 3219-5645( ) 0232-3219 SHMDT-J SHIMADZU TOKYO