Chempure TM 1. 2. 3. 3.1. OfficeXp-Word Office97-Word Office2000-Word Ctrl End Ctrl 3.2. Office-Word Office97-Word Ctrl End - 1 -

Chempure TM PN 51-Chemp/rev.A 1997 5

Chempure TM 1. 2. 3. 3.1. OfficeXp-Word Office97-Word Office2000-Word Ctrl End Ctrl 3.2. Office-Word Office97-Word Ctrl End - 1 -

1 Chempure TM Chempure TM Chempure TM CHEMISTRY CHEMISTRY 2 Chempure TM - 2 -

Rosemount Analytical, Uniloc Division 2400 Barranca Parkway Irvine, CA 92606 USA TEL: (800) 854-8257, (949) 757-8500 FAX: (949) 474-7250 3 3.1 3.1.1-3 -

1/2 0.5 LAMP PS 1 Amp 1 PUMP 1 Amp 1 XFMR 1 Amp 1 Pump On/Off Pump Norm/Hi On/Off Colorimeter Waste Drain Pan Pump Connector Heating Bath Connector Solenoid Valve #3 3# chemistry Pump Assembly Reaction Vessel Assembly Chemistry Module Tubing Quick-Disconnect Pump Tubing Harness Waste Tube Leak Detector 3.1.2 Cabinet Light Solenoid Valve Power Connectors Sample Solenoid Valve #1 Baseline/Standard Solenoid Valve #2 Multi-Stream Valve Panel - 4 -

Multi-Stream Connector Bulkhead Fitting 3-1 - 5 -

3-2 3.2 3.2.1 Thumbscrews Digital Display Status Panel 1 1 Sample Stream Indicator 3.2.2 man. multi-stream Enter auto cal man. Fullscale auto multi-stream man. Baseline - 6 -

set multi-stream hi alarm dec. loc. low alarm Power rec. f/s tube reset rec.zero leak LED calibration LED lamp LED ( ) pump tube LED 3-3 3.3-7 -

3.3.1 Keypad Panel Door Display Board CPU Board Multi-Stream and Multi-RS-232C CRS-232C Fault/Analog Power Board 3.3.2 CPU 3-4 CPU 3-5 / 20mA Adjust Set Screw 20 4mA Adjust Set Screw 4 5V Adjust Set Screw 5 0V Adjust Set Screw 0 Computer Memory Reset Switch - 8 -

3.3.3 / Leak Detector Adjust Set Screw 3.4 3-6 Colorimeter Source Lamp Interference Filter Assembly Sample Flow Cell Sample Flow Colorimeter Connector - 9 -

3-7 3.5 Pump Housing Pump Platen Assembly Reaction Vessel Assembly Chemistry Module Tubing Quick-Disconnect Colorimeter Inlet Tubing Thermometer Pump Drip Tray 3.6-10 -

3-8 3.7 / / - 11 -

3-9 / 3.8 Printer Interface Relay Output RS-232C Interface - 12 -

3-10 RS232-C 3.9 3-1 Intake/Regulating Valve Overflow Tube Sample Inlet Tube 1 Air Vent Waste Pipe - 13 -

3-11 4 4.1 4.1.1 168 111 / - 14 -

200 50 F 90 F 10 F = 10 80% 1. 4-1 6 2. 200 3. 3/8" 3/4" 3/8" 3/8" 4-1 4.2 1. 1/4" - 15 -

2. 3. 4.3 1. 2. 3-1 4.4 1. 4-2 IF-100 2. 3. 4. 1/4 a. b. c. 4.5 / 3-9 / - 16 -

4-2 - 17 -

4-3 4-4 0-5 / 4-20 - 18 -

1. / 2. 3. 4. / 3# Romex / 4.6 1. 3-1 2. 3. 4.7 1. 45 2. 4-4 3. 4. 4-5 5. 4-5 - 19 -

6. 90 4-4 7. 4-5 4.8 1. 4-6 2. 3. 4. 5. 6. - 20 -

4-6 4-7 1# 2# 4-8 3# - 21 -

4.9 1. 4-3 3-6 2. 3. 1# 4. SAMPLE 1# 4-7 3# 1. 3# NO 4-8 2. 3# C 4-6 3. 3# NC 4.10 1. 2. 3. 4. 2# 5. 6. 5 5.1 Chempure - 22 -

5.2 tube reset tube reset 5.3 1. 2. Enter 1. Dec.Loc. 2. 3. Enter 5.4 Chempure - 23 -

5-1 6 6.1 1. 0-50 C (30-122 F ) 2. 10-15ML/Min 3. 6.2 1. 2. 3. 4. 5. 6. Chemistry 6.3 1. - 24 -

2. 3. 6.4 1. 2. 3. CPU 4. 5. 6. 7. 20 5-7 6.5 30 45 Chemistry 7 Chempure - 25 -

7.1 12 48 1. 2. 3. normal 4. auto cal. 1. calibration LED auto cal man. baseline LED 2. 22 3. man. baseline LED man. fullscale LED 4. 22 5. man. fullscale LED 6. 7. auto reset( ) power 7.2 1. tube reset A 2. man.baseline 3. calibration LED man. baseline LED 4. - 26 -

7.3 1. tube reset A 2. man. fullscale 3. calibration LED man. fullscale LED 4. 7.4 15 8 8.1 1. 2. HI 5 3. 4. 8.2 1. 2. HI 5 3. 4. 5. - 27 -

6. 8.3 1. 2. 3. auto cal. 8.4 1. 2. 3. 4. auto cal. 8.5 1. 2. 3. 4. HI 5. 5 6. norm 7. 8. auto cal. 9 Chempure - 28 -

IF-100 9.1 0-5V 4-20mA / 3-9 9.1.1 1. rec.zero 0V 4mA 2. (enter) 3. rec.f/s 5V 20mA 4. (enter) 1. rec.zero 0V 4mA 2. CPU 3-4 (enter) 3. rec.f/s 5V 20mA 4. CPU 3-4 (enter) - 29 -

9-1 12 48 9-1 9.1.2 9-1 - 30 -

9.2 / 3-9 9-2 - 31 -

1. hi alarm 2. 3. enter ( ) 4. low alarm 5. 6. enter ( ) 1. hi alarm low alarm 2. enter ( ) 9.3 0-999 9.3.1 9.3.1.1 1. 2. 3. 4. 5. - 32 -

9.3.1.2 set multi-stream,auto. multi-stream man. multi-stream 1. CPU 2. 3. 4. CPU 9-3 5. 9-2 6. 9-3 7. RS-232C 9-3 8. 9-3 9. 9-3 - 33 -

9.3.2 1. 2. 3. 4. 5. 1# NO 6. 1. NO 2. 3. 9.3.2.1 4-6 1. 2. 3. 4. 5. 1/4 a) b) c) - 34 -

6. 9.3.3 1. _ set multi-stream 2.0000 stream 0 # 0-999 0 000 3.1015 1# 15 enter 15 enter 4.2015 2# 15 15 5.3015 3# 15 15 6. 015 7. set multi-stream sream1#( 1#) hi alarm enter low alarm enter 8. 015 15 0-35 -

9.3.4 9.3.4.1 auto cal. 1# 12 48 9.3.4.2 1. man. multi-stream 2. 1# enter 3. 4. a) man. multi-stream b) auto. multi-stream 9.4 IF-100 IF-100 IF-100 4 IF-100 9.5 RS232-C <CR> <LF> / - 36 -

9.5.1 9-2 NUL,STX,NUL= 00 02 00 / 25 7 5 9 7 YES NO NUL, EOT, NUL= 00 04 00 9.5.2 9-3 1200 8 0 1-37 -

9.5.3 RS232-C PIN * Active pins 9.5.4 RS232-C 1. CFA-1000 RS232-C CFA-1000 RS232-C CFA-1000 2. CFA-1000 3. - 38 -

4. 5. ANA-COM Return 6. Return M> 9-9 RS232-C 7. Control R 8 Return 8. Return M> 9.5.5 RS232-C RS232-C IBM PC 150 150 IBM PC 9-5 RS232-C RECFS RECZERO SETBLNO Q Q [ SETDECI ] SETVTIM 2# 20 SETVTIM 2 20 SETLAL 2# 50 SETLAL 2 50-39 -

SETHAL 1# 25 SETHAL 1 25 DISVALV AUTOVALV MANVALV, 3# MANVALV 3 SETDECI 1=XXX.X 2=XX.XX 4=X.XXX 8=.XXXX XX.XX SETDECI 2 MANBL MANFS SETCLO X X =0 =1 =2 =3 =4 24 1990 4 12 4 35 SETCLO 4900412163500 TIME PRININT 15 PRININT 15 DATA CALABOR 9.6 IBM PC - 40 -

9.6.1 PIN 9-6 PIN 9.7 9.7.1 1. Tube Reset Auto Multi 2. X =0 =1 =2 =3 =4 Enter 1991=92 1993=93 Enter 1 = 01 2 = 02 Enter - 41 -

1 = 01 28 = 28 Enter 24 8 00 Am = 8 1:00 Pm = 13 Enter 1 = 01 56 = 56 Enter 9.7.2 1. Tube Reset Dec. Loc 2. Tube Reset Manual Full scale 1999 10 Enter 9.7.3 PRN 0 9.8 9.8.1 9.8.2-42 -

10 Chempure 10.1 10.1.1. 1. 2. 10.1.2. 1. 2. 3. 4. - 43 -

10.1.3. 1. 12 2. 3. 1# 4. a) 0.5 b) c) 0.5 d) e) 10.1.4. 1. 11 A 11.1.1-44 -

- 45-20 / -LO- -HI - E-LO 0.5 0.5 E-HI PC auto cal.( ) 50-80 F 0.5 10

- 46-45

11.1.2 Front panel test tube reset hi alarm rec. zero Millivolts tube reset auto cal tube reset auto cal Gain tube reset rec. enter f/s Model number and prom version tube reset rec. enter zero 12 Chempure Rosemount Analytical, Uniloc Division 2400 Barranca Parkway Irvine, CA 92606 USA TEL: (800) 854-8257; (714) 757-8500 FAX: (714) 474-7250 12.1 1. 2. 3. 4. 5. - 47 -

12.1.1 1. 2. 3. 4. 5. 6. 12.1.2 1. 2. 3. 12.1.2 1. 2. 3. 12-1 - 48 -

12-2 12.2 12.2.1 1. 1# 2. 3. 3 4. 5. 12-3 6. 7. 1. 2. 3. 4. - 49 -

5. 6. 7. 8. 6 12-3 12-4 - 50 -

12.2.2 1. 1# 2. 3. 3 4. 5. 6. 7. 8. 9. 10. 11. 12. 13. 14. 12.3 1. 2. 3. 4. 5. 6. 7. 8. 12.4 3-1 1. 2. - 51 -

3. 4. 5. 6. 12-5 - 52 -

13 13-1 - 53 -

Chempure - 54 -

14 18" x 28" x 15" ( ) 126 57 176 80 115V 10%, 60 Hz ( 230V 10%) 10-15 ml/ minute 10 / 32-122 F - 55 -

50 F 104 F 10 F 80% 0-5 V, 500, 4-20 ma, 1200 3 250 1/10 3 30 - IBM 15 12 90 12 90 12 90-56 -

16 RMA (M.S.D.S.) Rosemount Analytical Inc. Uniloc Division 2400 Barranca Parkway Irvine, CA 92606-57 -

1... - 2-2... - 2-3... - 3-3.1...- 3-3.1.1... - 3-3.1.2... - 4-3.2...- 6-3.2.1... - 6-3.2.2... - 6-3.3...- 7-3.3.1... - 8-3.3.2 CPU... - 8-3.3.3 /... - 9-3.4...- 9-3.5...- 10-3.6...- 10-3.7 /...- 11-3.8...- 12-3.9...- 13-4... - 14-4.1...- 14-4.1.1... - 14-4.2...- 15-4.3...- 16-4.4...- 16-4.5...- 16 - - 1 -

... - 19-4.6...- 19-4.7...- 19-4.8...- 20-4.9...- 22-4.10...- 22-5... - 22-5.1...- 22-5.2...- 23-5.3...- 23-5.4...- 23-6... - 24-6.1...- 24-6.2...- 24-6.3...- 24-6.4...- 25-6.5...- 25-7... - 25-7.1...- 26-7.2...- 26-7.3...- 27-7.4...- 27-8... - 27-8.1...- 27-8.2...- 27-8.3...- 28-8.4...- 28-8.5...- 28 - - 2 -

9... - 28-9.1...- 29-9.1.1... - 29-9.1.2... - 30-9.2...- 31-9.3...- 32-9.3.1... - 32-9.3.1.1... - 32-9.3.1.2... - 33-9.3.2... - 34-9.3.2.1... - 34-9.3.3... - 35-9.3.4... - 36-9.3.4.1... - 36-9.3.4.2... - 36-9.4 IF-100...- 36-9.5...- 36-9.5.1... - 37-9.5.2... - 37-9.5.3 RS232-C PIN... - 38-9.5.4 RS232-C... - 38-9.5.5 RS232-C... - 39-9.6...- 40-9.6.1 PIN... - 41-9.7...- 41-9.7.1... - 41-9.7.2... - 42-9.7.3... - 42-9.8...- 42 - - 3 -

9.8.1... - 42-9.8.2... - 42-10... - 43-10.1...- 43-10.1.1.... - 43-10.1.2.... - 43-10.1.3.... - 44-10.1.4.... - 44-11... - 44-11.1.1... - 44-11.1.2... - 47-12... - 47-12.1...- 47-12.1.1... - 48-12.1.2... - 48-12.1.2... - 48-12.2...- 49-12.2.1... - 49-12.2.2... - 51-12.3...- 51-12.4...- 51-13... - 53-14... - 55-15... - 56-16... - 57 - - 4 -