,-,-,- : RP8, μm,.6 x mm : % MeCN/% mm KHPO ph at C : RP8, μm,.6 x mm : % MeCN/% mm KHPO ph at C (C8) TMS, >8, / m /g Å µm Grace

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1 Grace Davison Discovery Sciences Brochure #7

2 ,-,-,- : RP8, μm,.6 x mm : % MeCN/% mm KHPO ph at C : RP8, μm,.6 x mm : % MeCN/% mm KHPO ph at C (C8) TMS, >8, / m /g Å µm Grace Davison L C8 L Grace Smart Grace Grace Grace Alltech, Grom, Jones,Vydac Grace

3 N- P- Grace Smart 6 Grace Smart RP-8 : Grace Smart C8, m, x.6mm : H O :CH CN ( : 8 ) : L : UV, nm mau Grace Smart Min. C8 Luna C8 Inertsil ODS- Hypersil BDS C8 Kromasil - C8 C8,µm,.6 x mm ( 88 ).N KH PO,pH: CHCN (96:) µl.ml/min C UV, nm Hypersil BDS C8 Kromasil - C8 C8 Luna C8 Inertsil ODS- N/A (min) ( ) T f k'. k' ,, 8, 6,,,... Competitor C8 Competitor C8,-,-,-.. N,N ,-,-,- Competitor C8 C8

4 (U.S.P.).. (U.S.P.) Min. 6 8 Min. C8,µm,.6 x mm ( 88) HO ( HPO ph.): CH CN (6:) ml/min UV, nm µl C8,µm,.6 x mm ( 88).9% NaHPO (ph.): CH CN (:6).mL/min UV, 8nm C µl Min. C8,µm,.6 x mm ( 88) A:.M KHPO (ph.) B: CHCN (Time, %B): (,), (,6).mL/min UV, nm µl 6 7 Min. C8,µm,.6 x mm ( 88).M KHPO(pH.) : CHOH (97:).7mL/min UV, nm µl ,- 6 8 Min. 6 8 Min. C8,µm,.6 x mm ( 88) A:.M NHHPO ph. B: CHCN (Time, %B): (,), (,), (,), (,).ml/min UV, nm μl C8,µm,.6 x mm ( 88) A: % B: % (Time, %B): (,), (6,) (8,6), (,8).mL/min UV, 8nm µl

5 R R z q K Grace Smart Alltech ELSD. C.. A. B Folium Ginkgo > 888 C 6 6 A 869 B Bulbus Fritillariae Thunbergii > Min. CH OH : THF: H O( : : 6) µl.ml/min ELSD, > 778 adix Astragali 6 8 Min. CH CN : H O : (CH (7 : :.) CH ) NH µl.ml/min ELSD, 6 Fructus Kochiae > 67 Ic 6 8 Min. CH CN : H O( : 6) µl.ml/min ELSD, Rhizoma Anemarrhenae > Min. CH OH : H O: CH COOH (8 : :.) µl.ml/min ELSD, 6 Fructus Liquidambaris > 6 8 Min Min. CH OH : H O(9 : ) CH OH : H O: CH COOH (87 : :.) µl.ml/min ELSD, 8 µl.ml/min ELSD, 6

6 RP8 x RMB 88.6 x mm µm x mm µm x mm µm x mm µm 69 Grace Smart RP-8 Exmere Exsil Exsil Exsil Exsil-8 Exsil- Clasico Exsil-PLUS Avanti Avanti BDS Exsil- Exsil- Exsil- Å ml/g m /g > µ m.,,,.,,,,,,,,.,,,,,, Si C(TMS) C C6 C8 C8B C8AB ODS ODS- ODS- ODS-B ODS-AB Phenyl Phenyl() NH NH () CN CN() SAXX SCX X Quattro PAH HAAXX GRACESMART GRACE DAVISON DISCOVERY SCIENCES W.R.Grace&Co.-Conn. GRACE W.R.Grace&Co.-Conn. GRAPH-TITE,NO-SLIP SOFGRIP Alltech Associates,Inc. GRACE DAVISON DISCOVERY SCIENCES W.R.Grace&Co.-Conn. Alltech Associates,Inc. W.R.Grace&Co.-Conn. Alltech Associates, Inc. 7 GRACE Waukegan Rd. Brandstraat Brookhollow Avenue Deerfield, IL 6 B-96 Lokeren, Belgium Baulkham Hills Tel: Tel: New South Wales, Australia Fax: Fax: Tel: 6 contact.alltech@grace.com info-lokeren.alltech@grace.com Fax: 6 custcare-aust.discoverysciences@grace.com /7 #7 GEN

Grace Davison PLC L C8 L PLC GraceSmart RP8...,- 6.,- ( C8, DS ) 7.,- : GraceSmart RP8, μm, 0 x.6mm : 0% MeC 0% 0mM KP, p, C μm GracePure 0 A B

Grace Davison PLC L C8 L PLC GraceSmart RP8...,- 6.,- ( C8, DS ) 7.,- : GraceSmart RP8, μm, 0 x.6mm : 0% MeC 0% 0mM KP, p, C μm GracePure 0 A B Grace Davison Discovery Sciences GraceSmart Brochure #7 Grace Davison PLC L C8 L PLC. 0696. GraceSmart RP8...,- 6.,- ( C8, DS ) 7.,- : GraceSmart RP8, μm, 0 x.6mm : 0% MeC 0% 0mM KP, p, C μm GracePure