Alltech HPLC C8,, 0µm 00Å 6% Yes C8-WP µm 00Å 7% Yes C8-LL µm 00Å 9% Yes C8 C8-nuc µm 00Å 6% Yes AQ, µm 00Å % Yes 9% 00% C8,, 0µm 00Å 9% Yes C-WP µm 0

Size: px

Start display at page:

Download "Alltech HPLC C8,, 0µm 00Å 6% Yes C8-WP µm 00Å 7% Yes C8-LL µm 00Å 9% Yes C8 C8-nuc µm 00Å 6% Yes AQ, µm 00Å % Yes 9% 00% C8,, 0µm 00Å 9% Yes C-WP µm 0"

岚闻
7 years ago
Views:

1 LC/MS 7

2 Alltech HPLC C8,, 0µm 00Å 6% Yes C8-WP µm 00Å 7% Yes C8-LL µm 00Å 9% Yes C8 C8-nuc µm 00Å 6% Yes AQ, µm 00Å % Yes 9% 00% C8,, 0µm 00Å 9% Yes C-WP µm 00Å 6% Yes Phenyl, µm 00Å 7.% Yes Cyano, µm 00Å Yes Amino, µm 00Å No Silica,, 0µm 00Å

3 . Oxytetracycline Dihydrate. Tetracycline HCL. Meclocycline Sulfosalicylate Salt Ethotoin 6. Phenobarbital. Methsuximide. Mephenytoin. Carbamazepine 6. Diazepam Min. C8, µm, 00 x.6mm A: 0mM KHPO, ph.0 B: CHCN : 0 0 %B: 0.0mL/min UV at nm Min. Phenyl, µm, 0 x.6mm A: HO B: CHCN : %B: mL/min UV at nm USP XXII 768. Triazolam. Alprazolam Min. Silica, µm, 00 x.6mm CHCN:CHCl:i-BuOH:HO:Glacial HOAc (8:8:::0.0).0mL/min UV at nm C8, µm, 0 x.6mm HO:MeOH (0:60).0mL/min ELSD 77. DL--Hydroxy-- methoxy-mandelic Acid DL-. Homovanillic Acid. Vanillic Acid. Salicylic Acid. Benzoic Acid 7. Tripelennamine. Triprolidine. Cyclizine. Chlorcyclizine. Meclizine Min. C8, µm, 0 x.6mm 0mM KHPO, ph.:meoh (60:0).0mL/min UV at nm Min. C8, µm, 0 x.6mm A: 0mM KHPO, ph. B: CHCN : 0 0 %B: 70.mL/min UV at 0nm

4 88., -Dipyridyl, -. 8-Hydroxyquinoline 8-. Uracil. Pyridine. Phenol. N,N-Dimethylaniline N,N-. -Butylbenzoic Acid - 6. Toluene Min. C8, µm,0 x.6mm 0mM KHPO, ph.0: CHCN (0:60).0mL/min UV at nm 0 6 Min. C8, µm, 0 x.6mm mm KHPO, ph7.0:thf:meoh (0::).0mL/min UV at nm 60 C Gly-Tyr - 60 C. Val-Tyr-Val Met-Enkephalin -. Leu-Enkephalin. Angiotensin II C8, µm 0 x.6mm A: 0.% TFA in HO:CHCN (9:), B: 0.% TFA in HO:CHCN (:7) : 0 60 %B: 0.0mL/min Min Min. UV at 0nm

5 LC/MS Expedite MS Expedite MS 0mm 0mm.mm.6mm C8 Expedite µm 0 x.mm 86 Expedite µm 0 x.mm 80 8 µm 0 x.mm 89 8 µm 00 x.mm 8 7 µm 0 x.mm 8 78 Expedite µm 0 x.6mm Expedite µm 0 x.6mm 8 9 Phenyl Expedite µm 0 x.mm Expedite µm 0 x.mm µm 0 x.mm 8 7 µm 00 x.mm µm 0 x.mm Expedite µm 0 x.6mm Expedite µm 0 x.6mm 8 9 Silica Expedite µm 0 x.mm Expedite µm 0 x.mm 80 7 µm 00 x.mm 8 98 µm 0 x.mm 88 µm 0 x.mm Expedite µm 0 x.6mm Expedite µm 0 x.6mm Prep Columns PARTICLE INDUSTRY STANDARD 0mm PACKING SIZE LENGTH X ID PART NO. PRICE C8 µm 0 x 7mm µm 0 x 7mm 89 0 µm 0 x 0mm µm 0 x 0mm µm 0 x mm µm 0 x mm µm 0 x 0mm mm 0µm 0 x 0mm µm 0 x mm µm 0 x mm C8 µm 0 x 7mm µ m 0 x 7mm 8 0 Alltech Expedite MS µm 0 x 0mm LC/MS µm 0 x 0mm µm 0 x mm µm 0 x mm µm 0 x 0mm µm 0 x 0mm LC/MS Columns 0µm 0 x mm µm 0 x mm PARTICLE PACKING SIZE LENGTH X ID PART NO. PRICE Silica µm 0 x 7mm Solvent v Reducer Columns µ m 0 x 7mm µm 0 x 0mm 87 8 µm 0 x 0mm µm 0 x mm µm 0 x mm µm 0 x 0mm µm 0 x 0mm µm 0 x mm 8 9 0µm 0 x mm PARTICLE INDUSTRY STANDARD PACKING SIZE LENGTH X ID PART NO. PRICE C8 µm 0 x mm µm 0 x mm 80 8 µm 0 x mm 8 0 C8-LL µm 0 x mm 8 8 µm 0 x mm 8 0 C8 µm 0 x 7mm 86 7 Phenyl µm 0 x mm 87 0

6 Analytical Columns AQ INDUSTRY WATERS PARTICLE STANDARD INSTRUMENT. PRICE P. P PACKING SIZE LENGTH X ID PART NO ART NO RICE C8 µm 0 x.6mm 8 8 µm 00 x.6mm µm 0 x.6mm µm 0 x.6mm µm 0 x.6mm µm 0 x.6mm µm 0 x.6mm AQ µm 0 x.6mm µm 0 x.6mm µm 00 x.6mm µm 0 x.6mm C8-WP µm 0 x.6mm µm 0 x.6mm C8-LL µm 0 x.6mm µm 0 x.6mm C8 µm 0 x.6mm 8 8 µm 00 x.6mm µm 0 x.6mm µm 0 x.6mm µm 0 x.6mm µm 0 x.6mm µm 0 x.6mm C-WP µm 0 x.6mm µm 0 x.6mm Phenyl µm 0 x.6mm µm 00 x.6mm µm 0 x.6mm µm 0 x.6mm µm 0 x.6mm Cyano µm 0 x.6mm µm 00 x.6mm µm 0 x.6mm µm 0 x.6mm µm 0 x.6mm Amino µm 0 x.6mm µm 00 x.6mm µm 0 x.6mm µm 0 x.6mm µm 0 x.6mm Silica µm 0 x.6mm 8 69 µm 00 x.6mm µm 0 x.6mm µm 0 x.6mm µm 0 x.6mm µm 0 x.6mm % C8 C8 AQ 00% Min. AQ, µm, 0 x.6mm mm KHPO, ph.:chcn (98:) 0.7mL/min UV at nm 986. Cytidine Monophosphate (CMP). Uridine Monophosphate (UMP). Guanosine Monophosphate (GMP). Adenosine Monophosphate (AMP) 6

7 Rocket Rocket Columns PARTICLE P ACKING S IZE L ENGTH X ID P ART N O. P RICE C8 µm x 7mm µm x 7mm AQ µm x 7mm C8 µm x 7mm µm x 7mm Phenyl µm x 7mm Rocket 70% Cyano µm x 7mm µm x 7mm Amino µm x 7mm µm x 7mm 87 6 Silica µm x 7mm deacetylbaccatin III 0- III(0- III). Baccatin III III ( III). 7-xylosyl-0-deacetyltaxol B B. Taxinine M M. 7-xylosyl-0-deacetyltaxol xylosyl-0-deacetyltaxol C C 7. 0-deacetyltaxol xylosyltaxol 7-9. Cephalomannine (Taxol B) ( B) 0. 7-epi-0-deacetyltaxol Taxol. Taxol 7 C C. 7-epitaxol, Myricetin. Quercetin. Apigenin. Kaempferol Min. Phenyl Rocket, µm, x 7mm 0.0% TFA in HO:MeOH:CHCN (0:9:).mL/min UV at 0nm 0 Min. C8 Rocket, µm, x 7mm 0.% TFA in HO, ph 0.9:0.% TFA in CHCN(6:).mL/min ELSD Validation Kits C8 C8 µ m µ m C8 C8 Validation Kits DESCRIPTION PART NO. PRICE C8 Method Validation Kits 00 x.6mm, µm Kit ( Columns from Different Batches) x.6mm, µm Kit ( Columns from Different Batches) 0 x.6mm, µm Kit ( Columns from Different Batches) 098 7

8 Guard All-Guard All-Guard DESCRIPTION PARTICLE SIZE LENGTH X ID QTY PART NO. PRICE C8 µm 7. x.mm µm 7. x.0mm µm 7. x.6mm C8-WP µm 7. x.mm 96 8 AQ µm 7. x.mm 96 C-WP µm 7. x.6mm 96 Prep-Guard Direct-Connect DESCRIPTION LENGTH XID Q TY PART NO. PRICE C8-LL µm 7. x.mm 96 µm 7. x.0mm C8 x 7mm µm 7. x.6mm C8 x 7mm Silica x 7mm C8 µm 7. x.mm 96 µm 7. x.0mm µm 7. x.6mm Direct-Connect Ea Phenyl µm 7. x.mm µm 7. x.0mm µm 7. x.6mm Cyano µm 7. x.6mm Amino µm 7. x.6mm Silica µm 7. x.mm Direct-Connect µm 7. x.6mm Direct-Connect All-Guard Ea Alltech,, Prevail, Grom, Jones Chromatography, Flexit, MODcol 和 Vydac 是 Alltech Associates, Inc 的商标 GRACE, GRACE DAVISON, DAVISON 和 DAVISIL 是 W. R. Grace & Co.-Conn 的注册商标 Alltech Associates, Inc 是 W. R. Grace & Co.-Conn. 全资子公司,Grace Davison 是 W. R. Grace & Co.-Conn. 的一个业务部门, 格雷斯的全球总部位于美国马里兰州的哥伦比亚市,Grace Drive 700,0

,-,-,- : RP8, μm,.6 x mm : % MeCN/% mm KHPO ph at C : RP8, μm,.6 x mm : % MeCN/% mm KHPO ph at C (C8) TMS, >8, / m /g Å µm Grace

Grace Davison Discovery Sciences Brochure #7 ..... 6. 7. 696,-,-,- : RP8, μm,.6 x mm : % MeCN/% mm KHPO ph at C : RP8, μm,.6 x mm : % MeCN/% mm KHPO ph at C.... 69 (C8) TMS, >8, / m /g Å µm Grace Davison